####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_as500 _audit_block_doi 10.5517/ccdc.csd.cc266gfb _database_code_depnum_ccdc_archive 'CCDC 2032001' loop_ _citation_id _citation_doi _citation_year 1 10.1021/acs.joc.0c02561 2021 loop_ _audit_author_name _audit_author_address 'Sergey Belyakov' ;Latvian Institute of Organic Synthesis Latvia ; _audit_update_record ; 2020-09-14 deposited with the CCDC. 2022-01-21 downloaded from the CCDC. ; _audit_creation_date 2020-04-15 _audit_creation_method ; Olex2 1.2-ac4 (compiled 2018.05.17 svn.r3504 for Rigaku Oxford Diffraction, GUI svn.r5492) ; _shelx_SHELXL_version_number 2018/3 _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C17 H19 Cl F S, B F4' _chemical_formula_sum 'C17 H19 B Cl F5 S' _chemical_formula_weight 396.64 _chemical_melting_point ? _chemical_oxdiff_formula 'C136 H152 B8 Cl8 F40 S8' _chemical_oxdiff_usercomment 'from Janis Velix' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_H-M_alt 'I 1 2/a 1' _space_group_name_Hall '-I 2ya' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' _cell_length_a 17.80457(19) _cell_length_b 7.60222(6) _cell_length_c 27.7595(3) _cell_angle_alpha 90 _cell_angle_beta 108.4869(11) _cell_angle_gamma 90 _cell_volume 3563.47(6) _cell_formula_units_Z 8 _cell_measurement_reflns_used 16202 _cell_measurement_temperature 150.0(1) _cell_measurement_theta_max 77.1950 _cell_measurement_theta_min 3.3420 _shelx_estimated_absorpt_T_max 0.820 _shelx_estimated_absorpt_T_min 0.644 _exptl_absorpt_coefficient_mu 3.431 _exptl_absorpt_correction_T_max 0.85019 _exptl_absorpt_correction_T_min 0.60168 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.74a (Rigaku Oxford Diffraction, 2020) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour Colourless _exptl_crystal_density_diffrn 1.479 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description 'Prism ' _exptl_crystal_F_000 1632 _exptl_crystal_size_max 0.14 _exptl_crystal_size_mid 0.13 _exptl_crystal_size_min 0.06 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0285 _diffrn_reflns_av_unetI/netI 0.0206 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.991 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 6 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 35 _diffrn_reflns_limit_l_min -35 _diffrn_reflns_number 19685 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.991 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 77.417 _diffrn_reflns_theta_min 3.357 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 150.0(1) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.991 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 90.00 115.00 0.50 0.21 -- 47.95 77.00 -30.00 50 2 \w 92.00 128.00 0.50 0.80 -- 107.75 61.00-180.00 72 3 \w 106.00 131.00 0.50 0.80 -- 107.75 30.00-150.00 50 4 \w 97.00 131.00 0.50 0.80 -- 107.75 45.00-120.00 68 5 \w 152.00 177.00 0.50 0.80 -- 107.75 30.00-150.00 50 6 \w 128.00 173.00 0.50 0.80 -- 107.75 77.00 -60.00 90 7 \w 100.00 176.00 0.50 0.80 -- 107.75 45.00 -60.00 152 8 \w 106.00 132.00 0.50 0.80 -- 107.75 15.00-150.00 52 9 \w 133.00 165.00 0.50 0.80 -- 107.75 15.00-150.00 64 10 \w 119.00 178.00 0.50 0.80 -- 107.75 13.00-107.00 118 11 \w 113.00 145.00 0.50 0.80 -- 107.75 30.00 -30.00 64 12 \w 132.00 158.00 0.50 0.80 -- 107.75 45.00 120.00 52 13 \w 53.00 79.00 0.50 0.21 -- 47.95 13.00-107.00 52 14 \w 3.00 36.00 0.50 0.21 -- 47.95 -19.00 -90.00 66 15 \w 96.00 123.00 0.50 0.80 -- 107.75 125.00 30.00 54 16 \w 110.00 135.00 0.50 0.80 -- 107.75 125.00-120.00 50 17 \w 84.00 110.00 0.50 0.80 -- 107.75 -88.00-103.37 52 18 \w 40.00 89.00 0.50 0.21 -- 47.95-125.00 0.00 98 19 \w 35.00 64.00 0.50 0.80 -- 107.75-125.00 150.00 58 20 \w 87.00 112.00 0.50 0.80 -- 107.75-125.00 150.00 50 21 \w 84.00 109.00 0.50 0.80 -- 107.75-125.00 120.00 50 22 \w 39.00 78.00 0.50 0.80 -- 107.75-125.00 120.00 78 23 \w 81.00 106.00 0.50 0.80 -- 107.75 -94.00 -30.00 50 24 \w 86.00 111.00 0.50 0.80 -- 107.75-125.00 -90.00 50 25 \w 79.00 107.00 0.50 0.80 -- 107.75-125.00-150.00 56 26 \w 81.00 108.00 0.50 0.80 -- 107.75-125.00-180.00 54 27 \w 72.00 105.00 0.50 0.80 -- 107.75 -94.00-180.00 66 28 \w 59.00 85.00 0.50 0.80 -- 107.75 -94.00-150.00 52 29 \w 37.00 67.00 0.50 0.80 -- 107.75 -94.00 -90.00 60 30 \w 54.00 106.00 0.50 0.80 -- 107.75 -94.00-120.00 104 31 \w 60.00 105.00 0.50 0.80 -- 107.75 -94.00 -60.00 90 32 \w 72.00 103.00 0.50 0.80 -- 107.75 -94.00 -90.00 62 33 \w 37.00 62.00 0.50 0.80 -- 107.75 -94.00 -30.00 50 34 \w 35.00 60.00 0.50 0.80 -- 107.75 -94.00 0.00 50 35 \w 47.00 95.00 0.50 0.80 -- 107.75 -94.00 150.00 96 36 \w 77.00 103.00 0.50 0.80 -- 107.75 -94.00 0.00 52 37 \w 45.00 75.00 0.50 0.80 -- 107.75 -88.00-103.37 60 38 \w 39.00 64.00 0.50 0.80 -- 107.75 -77.00 -90.00 50 39 \w 38.00 64.00 0.50 0.80 -- 107.75 -61.00 -90.00 52 40 \w 35.00 60.00 0.50 0.80 -- 107.75 -61.00-180.00 50 41 \w 35.00 63.00 0.50 0.80 -- 107.75 -61.00 0.00 56 42 \w 38.00 68.00 0.50 0.80 -- 107.75 -61.00 90.00 60 43 \w -119.00 -88.00 0.50 0.21 -- -47.95 -77.00 90.00 62 44 \w -144.00-111.00 0.50 0.80 -- -86.25 -13.00 80.00 66 45 \w -121.00 -35.00 0.50 0.21 -- -47.95 -13.00 80.00 172 46 \w -45.00 16.00 0.50 0.21 -- -47.95 13.00-107.00 122 47 \w -48.00 -23.00 0.50 0.80 -- -86.25 13.00-107.00 50 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0384700000 _diffrn_orient_matrix_UB_12 -0.0328118000 _diffrn_orient_matrix_UB_13 0.0416681000 _diffrn_orient_matrix_UB_21 -0.0827116000 _diffrn_orient_matrix_UB_22 0.0115415000 _diffrn_orient_matrix_UB_23 -0.0400555000 _diffrn_orient_matrix_UB_31 0.0015554000 _diffrn_orient_matrix_UB_32 -0.1996594000 _diffrn_orient_matrix_UB_33 -0.0091744000 _diffrn_oxdiff_digest_frames ; 01d880a6b66755131ba325f30e6b8f3c9d000504563 ; _diffrn_oxdiff_digest_hkl ; 013cd388a12264be605654007b9a69b13e8c43 ; _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3602 _reflns_number_total 3764 _reflns_odcompleteness_completeness 100.00 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.40.74a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.40.74a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.40.74a (Rigaku OD, 2020)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve (Bourhis et al., 2015)' _refine_diff_density_max 1.102 _refine_diff_density_min -0.581 _refine_diff_density_rms 0.062 _refine_ls_extinction_coef 0.00037(7) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.081 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 243 _refine_ls_number_reflns 3764 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0470 _refine_ls_R_factor_gt 0.0458 _refine_ls_restrained_S_all 1.081 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0599P)^2^+6.7647P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1232 _refine_ls_wR_factor_ref 0.1243 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Others Fixed Sof: F2(0.8) F4(0.8) F3(0.8) F2A(0.2) F3A(0.2) F4A(0.2) 3.a Secondary CH2 refined with riding coordinates: C18(H18A,H18B) 3.b Aromatic/amide H refined with riding coordinates: C6(H6), C16(H16), C13(H13), C15(H15), C12(H12) 3.c Idealised Me refined as rotating group: C7(H7A,H7B,H7C), C8(H8A,H8B,H8C), C10(H10A,H10B,H10C), C9(H9A,H9B,H9C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S 0.32528(3) 0.32388(6) 0.59853(2) 0.02257(15) Uani 1 1 d . . . . . Cl17 Cl 0.49031(4) -0.32506(8) 0.53768(2) 0.0499(2) Uani 1 1 d . . . . . F19 F 0.19177(8) 0.3041(2) 0.52638(5) 0.0490(4) Uani 1 1 d . . . . . F1 F 0.11273(9) 0.6400(2) 0.60742(7) 0.0538(4) Uani 1 1 d . . . . . C1 C 0.34808(11) 0.2986(2) 0.66570(7) 0.0227(4) Uani 1 1 d . . . . . C6 C 0.32248(11) 0.1483(3) 0.68417(7) 0.0257(4) Uani 1 1 d . . . . . H6 H 0.296714 0.059865 0.661889 0.031 Uiso 1 1 calc R . . . . C11 C 0.36565(11) 0.1339(3) 0.57804(7) 0.0237(4) Uani 1 1 d . . . . . F2 F 0.24365(12) 0.6729(3) 0.64210(10) 0.0685(7) Uani 0.8 1 d . . P . . F4 F 0.16964(12) 0.9093(2) 0.60637(13) 0.0773(9) Uani 0.8 1 d . . P . . C5 C 0.33532(11) 0.1298(3) 0.73589(7) 0.0272(4) Uani 1 1 d . . . . . C4 C 0.37524(11) 0.2649(3) 0.76851(7) 0.0273(4) Uani 1 1 d . . . . . C16 C 0.44221(12) 0.1561(3) 0.57612(8) 0.0301(4) Uani 1 1 d . . . . . H16 H 0.467396 0.264592 0.583474 0.036 Uiso 1 1 calc R . . . . C13 C 0.36370(14) -0.1651(3) 0.55164(8) 0.0331(4) Uani 1 1 d . . . . . H13 H 0.337751 -0.272095 0.542585 0.040 Uiso 1 1 calc R . . . . C2 C 0.39038(10) 0.4330(3) 0.69713(7) 0.0248(4) Uani 1 1 d . . . . . C3 C 0.40392(11) 0.4130(3) 0.74968(7) 0.0278(4) Uani 1 1 d . . . . . C15 C 0.48030(12) 0.0132(3) 0.56299(8) 0.0356(5) Uani 1 1 d . . . . . H15 H 0.531780 0.024290 0.561946 0.043 Uiso 1 1 calc R . . . . C14 C 0.44115(13) -0.1445(3) 0.55159(7) 0.0334(5) Uani 1 1 d . . . . . C7 C 0.42134(13) 0.5918(3) 0.67698(8) 0.0369(5) Uani 1 1 d . . . . . H7A H 0.410738 0.579425 0.641020 0.055 Uiso 1 1 calc GR . . . . H7B H 0.477415 0.601508 0.693409 0.055 Uiso 1 1 calc GR . . . . H7C H 0.395580 0.695560 0.683683 0.055 Uiso 1 1 calc GR . . . . C18 C 0.21806(11) 0.2874(3) 0.57781(7) 0.0279(4) Uani 1 1 d . . . . . H18A H 0.206271 0.170753 0.587635 0.033 Uiso 1 1 calc R . . . . H18B H 0.192520 0.373360 0.593238 0.033 Uiso 1 1 calc R . . . . C12 C 0.32551(12) -0.0237(3) 0.56540(7) 0.0293(4) Uani 1 1 d . . . . . H12 H 0.273844 -0.034816 0.566085 0.035 Uiso 1 1 calc R . . . . F3 F 0.1917(2) 0.6859(3) 0.56078(10) 0.0872(9) Uani 0.8 1 d . . P . . C8 C 0.44931(14) 0.5524(3) 0.78629(9) 0.0416(5) Uani 1 1 d . . . . . H8A H 0.421103 0.582152 0.809450 0.062 Uiso 1 1 calc GR . . . . H8B H 0.454814 0.655344 0.767655 0.062 Uiso 1 1 calc GR . . . . H8C H 0.500830 0.508234 0.804990 0.062 Uiso 1 1 calc GR . . . . C10 C 0.30576(14) -0.0332(3) 0.75503(9) 0.0395(5) Uani 1 1 d . . . . . H10A H 0.266875 -0.000964 0.770755 0.059 Uiso 1 1 calc GR . . . . H10B H 0.349274 -0.091281 0.779437 0.059 Uiso 1 1 calc GR . . . . H10C H 0.282314 -0.111066 0.727077 0.059 Uiso 1 1 calc GR . . . . C9 C 0.38676(14) 0.2518(3) 0.82478(8) 0.0388(5) Uani 1 1 d . . . . . H9A H 0.355445 0.340182 0.834141 0.058 Uiso 1 1 calc GR . . . . H9B H 0.441634 0.269481 0.843569 0.058 Uiso 1 1 calc GR . . . . H9C H 0.370504 0.137482 0.832323 0.058 Uiso 1 1 calc GR . . . . B1 B 0.17695(14) 0.7346(3) 0.60596(9) 0.0331(5) Uani 1 1 d . . . . . F2A F 0.2417(5) 0.6656(11) 0.6081(4) 0.056(2) Uiso 0.2 1 d . . P . . F3A F 0.1543(4) 0.8553(9) 0.5661(2) 0.0363(14) Uiso 0.2 1 d . . P . . F4A F 0.1797(5) 0.8511(11) 0.6503(3) 0.0532(18) Uiso 0.2 1 d . . P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.0252(2) 0.0228(2) 0.0195(2) 0.00185(15) 0.00681(17) -0.00017(15) Cl17 0.0550(4) 0.0523(4) 0.0413(3) -0.0062(2) 0.0137(3) 0.0259(3) F19 0.0345(7) 0.0868(11) 0.0211(6) -0.0074(6) 0.0023(5) 0.0071(7) F1 0.0380(7) 0.0416(8) 0.0795(11) 0.0092(7) 0.0156(7) -0.0111(6) C1 0.0222(8) 0.0260(9) 0.0196(8) 0.0019(7) 0.0064(7) 0.0013(7) C6 0.0252(9) 0.0254(9) 0.0260(9) 0.0009(7) 0.0073(7) -0.0011(7) C11 0.0271(9) 0.0268(9) 0.0177(8) 0.0028(7) 0.0078(7) 0.0034(7) F2 0.0387(10) 0.0793(16) 0.0712(16) 0.0228(12) -0.0055(10) 0.0037(10) F4 0.0452(11) 0.0249(9) 0.168(3) -0.0065(12) 0.0430(14) -0.0043(8) C5 0.0250(9) 0.0313(9) 0.0273(9) 0.0072(8) 0.0110(7) 0.0048(7) C4 0.0243(8) 0.0370(10) 0.0216(9) 0.0028(7) 0.0087(7) 0.0097(8) C16 0.0267(9) 0.0366(11) 0.0269(9) 0.0007(8) 0.0084(7) 0.0001(8) C13 0.0434(12) 0.0289(10) 0.0288(10) -0.0007(8) 0.0142(9) 0.0024(8) C2 0.0214(8) 0.0273(9) 0.0251(9) -0.0004(7) 0.0066(7) -0.0006(7) C3 0.0226(8) 0.0347(10) 0.0248(9) -0.0035(8) 0.0058(7) 0.0025(7) C15 0.0269(9) 0.0507(13) 0.0295(10) -0.0004(9) 0.0095(8) 0.0070(9) C14 0.0396(11) 0.0395(11) 0.0205(9) 0.0017(8) 0.0087(8) 0.0152(9) C7 0.0390(11) 0.0349(11) 0.0341(11) -0.0014(9) 0.0079(9) -0.0143(9) C18 0.0231(8) 0.0358(10) 0.0234(9) -0.0035(8) 0.0054(7) 0.0038(8) C12 0.0321(10) 0.0296(10) 0.0288(9) -0.0001(8) 0.0135(8) 0.0001(8) F3 0.144(3) 0.0740(16) 0.0599(14) -0.0193(12) 0.0557(17) -0.0439(16) C8 0.0433(12) 0.0480(13) 0.0303(10) -0.0120(10) 0.0074(9) -0.0068(10) C10 0.0452(12) 0.0379(12) 0.0391(11) 0.0141(9) 0.0186(10) 0.0014(10) C9 0.0431(12) 0.0527(14) 0.0229(9) 0.0038(9) 0.0137(9) 0.0133(10) B1 0.0310(11) 0.0305(11) 0.0340(12) 0.0037(9) 0.0050(9) -0.0042(9) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 C1 1.7885(18) . ? S1 C11 1.7850(19) . ? S1 C18 1.832(2) . ? Cl17 C14 1.736(2) . ? F19 C18 1.360(2) . ? F1 B1 1.362(3) . ? C1 C6 1.387(3) . ? C1 C2 1.398(3) . ? C6 H6 0.9300 . ? C6 C5 1.387(3) . ? C11 C16 1.391(3) . ? C11 C12 1.382(3) . ? F2 B1 1.371(3) . ? F2 F2A 0.934(9) . ? F4 B1 1.335(3) . ? F4 F3A 1.140(7) . ? F4 F4A 1.255(9) . ? C5 C4 1.404(3) . ? C5 C10 1.507(3) . ? C4 C3 1.404(3) . ? C4 C9 1.513(3) . ? C16 H16 0.9300 . ? C16 C15 1.389(3) . ? C13 H13 0.9300 . ? C13 C14 1.388(3) . ? C13 C12 1.389(3) . ? C2 C3 1.410(3) . ? C2 C7 1.506(3) . ? C3 C8 1.513(3) . ? C15 H15 0.9300 . ? C15 C14 1.372(3) . ? C7 H7A 0.9600 . ? C7 H7B 0.9600 . ? C7 H7C 0.9600 . ? C18 H18A 0.9700 . ? C18 H18B 0.9700 . ? C12 H12 0.9300 . ? F3 B1 1.410(3) . ? F3 F2A 1.342(10) . ? F3 F3A 1.479(7) . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? C9 H9A 0.9600 . ? C9 H9B 0.9600 . ? C9 H9C 0.9600 . ? B1 F2A 1.250(9) . ? B1 F3A 1.396(7) . ? B1 F4A 1.504(9) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 S1 C18 100.40(9) . . ? C11 S1 C1 105.30(8) . . ? C11 S1 C18 105.20(9) . . ? C6 C1 S1 118.77(14) . . ? C6 C1 C2 123.11(17) . . ? C2 C1 S1 118.11(14) . . ? C1 C6 H6 120.0 . . ? C1 C6 C5 120.00(18) . . ? C5 C6 H6 120.0 . . ? C16 C11 S1 114.35(15) . . ? C12 C11 S1 123.66(14) . . ? C12 C11 C16 121.99(18) . . ? F2A F2 B1 62.3(6) . . ? F3A F4 B1 68.1(4) . . ? F3A F4 F4A 137.9(6) . . ? F4A F4 B1 70.9(4) . . ? C6 C5 C4 118.50(18) . . ? C6 C5 C10 119.10(19) . . ? C4 C5 C10 122.40(18) . . ? C5 C4 C9 119.54(19) . . ? C3 C4 C5 121.05(17) . . ? C3 C4 C9 119.41(19) . . ? C11 C16 H16 120.6 . . ? C15 C16 C11 118.7(2) . . ? C15 C16 H16 120.6 . . ? C14 C13 H13 120.5 . . ? C14 C13 C12 119.1(2) . . ? C12 C13 H13 120.5 . . ? C1 C2 C3 116.64(17) . . ? C1 C2 C7 122.82(17) . . ? C3 C2 C7 120.54(17) . . ? C4 C3 C2 120.60(18) . . ? C4 C3 C8 119.46(18) . . ? C2 C3 C8 119.94(19) . . ? C16 C15 H15 120.4 . . ? C14 C15 C16 119.29(19) . . ? C14 C15 H15 120.4 . . ? C13 C14 Cl17 118.83(18) . . ? C15 C14 Cl17 119.15(17) . . ? C15 C14 C13 122.02(19) . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7B 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? S1 C18 H18A 110.3 . . ? S1 C18 H18B 110.3 . . ? F19 C18 S1 107.04(13) . . ? F19 C18 H18A 110.3 . . ? F19 C18 H18B 110.3 . . ? H18A C18 H18B 108.6 . . ? C11 C12 C13 118.81(19) . . ? C11 C12 H12 120.6 . . ? C13 C12 H12 120.6 . . ? B1 F3 F3A 57.7(3) . . ? F2A F3 B1 54.0(4) . . ? F2A F3 F3A 100.5(5) . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10B 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9B 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? F1 B1 F2 109.8(2) . . ? F1 B1 F3 106.4(2) . . ? F1 B1 F3A 109.6(3) . . ? F1 B1 F4A 95.5(4) . . ? F2 B1 F3 101.4(3) . . ? F2 B1 F3A 140.4(3) . . ? F2 B1 F4A 78.9(4) . . ? F4 B1 F1 116.1(2) . . ? F4 B1 F2 113.5(2) . . ? F4 B1 F3 108.4(2) . . ? F4 B1 F3A 49.3(3) . . ? F4 B1 F4A 52.1(3) . . ? F3 B1 F4A 156.2(4) . . ? F2A B1 F1 123.1(5) . . ? F2A B1 F2 41.4(4) . . ? F2A B1 F4 120.5(4) . . ? F2A B1 F3 60.2(5) . . ? F2A B1 F3A 110.2(5) . . ? F2A B1 F4A 114.6(6) . . ? F3A B1 F3 63.6(3) . . ? F3A B1 F4A 100.8(5) . . ? F2 F2A F3 141.5(9) . . ? F2 F2A B1 76.3(6) . . ? B1 F2A F3 65.8(5) . . ? F4 F3A F3 115.8(5) . . ? F4 F3A B1 62.6(3) . . ? B1 F3A F3 58.7(3) . . ? F4 F4A B1 57.0(4) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag S1 C1 C6 C5 -176.27(14) . . . . ? S1 C1 C2 C3 176.93(13) . . . . ? S1 C1 C2 C7 -3.7(3) . . . . ? S1 C11 C16 C15 176.91(15) . . . . ? S1 C11 C12 C13 -177.74(15) . . . . ? F1 B1 F2A F2 -82.5(6) . . . . ? F1 B1 F2A F3 90.9(5) . . . . ? F1 B1 F3A F4 108.0(3) . . . . ? F1 B1 F3A F3 -99.1(3) . . . . ? F1 B1 F4A F4 -119.0(3) . . . . ? C1 S1 C11 C16 -92.80(15) . . . . ? C1 S1 C11 C12 86.68(17) . . . . ? C1 S1 C18 F19 179.61(14) . . . . ? C1 C6 C5 C4 -0.7(3) . . . . ? C1 C6 C5 C10 178.96(18) . . . . ? C1 C2 C3 C4 -0.5(3) . . . . ? C1 C2 C3 C8 179.92(18) . . . . ? C6 C1 C2 C3 -2.4(3) . . . . ? C6 C1 C2 C7 177.02(19) . . . . ? C6 C5 C4 C3 -2.0(3) . . . . ? C6 C5 C4 C9 177.28(17) . . . . ? C11 S1 C1 C6 -56.78(17) . . . . ? C11 S1 C1 C2 123.86(15) . . . . ? C11 S1 C18 F19 -71.25(15) . . . . ? C11 C16 C15 C14 1.0(3) . . . . ? F2 B1 F2A F3 173.5(7) . . . . ? F2 B1 F3A F4 -77.5(6) . . . . ? F2 B1 F3A F3 75.4(6) . . . . ? F2 B1 F4A F4 131.9(4) . . . . ? F4 B1 F2A F2 91.7(6) . . . . ? F4 B1 F2A F3 -94.8(4) . . . . ? F4 B1 F3A F3 152.9(4) . . . . ? C5 C4 C3 C2 2.7(3) . . . . ? C5 C4 C3 C8 -177.72(18) . . . . ? C16 C11 C12 C13 1.7(3) . . . . ? C16 C15 C14 Cl17 -177.46(15) . . . . ? C16 C15 C14 C13 1.5(3) . . . . ? C2 C1 C6 C5 3.1(3) . . . . ? C14 C13 C12 C11 0.7(3) . . . . ? C7 C2 C3 C4 -179.89(18) . . . . ? C7 C2 C3 C8 0.5(3) . . . . ? C18 S1 C1 C6 52.28(17) . . . . ? C18 S1 C1 C2 -127.07(15) . . . . ? C18 S1 C11 C16 161.63(14) . . . . ? C18 S1 C11 C12 -18.89(18) . . . . ? C12 C11 C16 C15 -2.6(3) . . . . ? C12 C13 C14 Cl17 176.57(16) . . . . ? C12 C13 C14 C15 -2.3(3) . . . . ? F3 B1 F2A F2 -173.5(7) . . . . ? F3 B1 F3A F4 -152.9(4) . . . . ? F3 B1 F4A F4 38.8(11) . . . . ? C10 C5 C4 C3 178.27(18) . . . . ? C10 C5 C4 C9 -2.4(3) . . . . ? C9 C4 C3 C2 -176.66(17) . . . . ? C9 C4 C3 C8 3.0(3) . . . . ? _shelx_res_file ; TITL as500_a.res in I2/a as500.res created by SHELXL-2018/3 at 00:15:49 on 15-Apr-2020 REM Old TITL AS500 in I2/a REM SHELXT solution in I2/a REM R1 0.209, Rweak 0.009, Alpha 0.040, Orientation as input REM Formula found by SHELXT: C20 B F1 Cl2 CELL 1.54184 17.804573 7.602221 27.759457 90 108.4869 90 ZERR 8 0.000188 0.000058 0.000292 0 0.0011 0 LATT 2 SYMM 0.5-X,+Y,-Z SFAC C H B Cl F S UNIT 144 152 8 8 40 8 L.S. 3 PLAN 7 SIZE 0.14 0.13 0.06 CONF BOND $H MORE -1 fmap 2 acta REM REM REM WGHT 0.059900 6.764700 EXTI 0.000366 FVAR 2.92852 S1 6 0.325277 0.323883 0.598531 11.00000 0.02517 0.02281 = 0.01954 0.00185 0.00681 -0.00017 CL17 4 0.490314 -0.325057 0.537677 11.00000 0.05495 0.05235 = 0.04125 -0.00622 0.01374 0.02587 F19 5 0.191770 0.304054 0.526380 11.00000 0.03451 0.08680 = 0.02113 -0.00740 0.00232 0.00709 F1 5 0.112732 0.640008 0.607421 11.00000 0.03797 0.04163 = 0.07952 0.00923 0.01556 -0.01113 C1 1 0.348083 0.298582 0.665703 11.00000 0.02225 0.02605 = 0.01957 0.00186 0.00637 0.00126 C6 1 0.322481 0.148274 0.684174 11.00000 0.02518 0.02540 = 0.02596 0.00089 0.00730 -0.00114 AFIX 43 H6 2 0.296714 0.059865 0.661889 11.00000 -1.20000 AFIX 0 C11 1 0.365649 0.133866 0.578041 11.00000 0.02711 0.02681 = 0.01775 0.00277 0.00784 0.00340 F2 5 0.243648 0.672918 0.642096 10.80000 0.03867 0.07933 = 0.07124 0.02284 -0.00549 0.00367 F4 5 0.169635 0.909315 0.606366 10.80000 0.04521 0.02494 = 0.16823 -0.00647 0.04302 -0.00428 C5 1 0.335318 0.129849 0.735893 11.00000 0.02498 0.03133 = 0.02731 0.00717 0.01101 0.00476 C4 1 0.375235 0.264904 0.768514 11.00000 0.02428 0.03697 = 0.02159 0.00280 0.00869 0.00974 C16 1 0.442205 0.156112 0.576115 11.00000 0.02675 0.03661 = 0.02693 0.00071 0.00840 0.00009 AFIX 43 H16 2 0.467396 0.264592 0.583474 11.00000 -1.20000 AFIX 0 C13 1 0.363703 -0.165080 0.551640 11.00000 0.04344 0.02888 = 0.02882 -0.00067 0.01424 0.00238 AFIX 43 H13 2 0.337751 -0.272095 0.542585 11.00000 -1.20000 AFIX 0 C2 1 0.390384 0.432973 0.697128 11.00000 0.02141 0.02733 = 0.02505 -0.00044 0.00664 -0.00059 C3 1 0.403923 0.412958 0.749685 11.00000 0.02258 0.03469 = 0.02481 -0.00354 0.00581 0.00245 C15 1 0.480301 0.013210 0.562993 11.00000 0.02689 0.05070 = 0.02946 -0.00036 0.00949 0.00700 AFIX 43 H15 2 0.531780 0.024290 0.561946 11.00000 -1.20000 AFIX 0 C14 1 0.441153 -0.144508 0.551590 11.00000 0.03958 0.03953 = 0.02050 0.00174 0.00871 0.01523 C7 1 0.421336 0.591765 0.676984 11.00000 0.03902 0.03489 = 0.03414 -0.00137 0.00788 -0.01428 AFIX 137 H7A 2 0.410738 0.579425 0.641020 11.00000 -1.50000 H7B 2 0.477415 0.601508 0.693409 11.00000 -1.50000 H7C 2 0.395580 0.695560 0.683683 11.00000 -1.50000 AFIX 0 C18 1 0.218064 0.287384 0.577813 11.00000 0.02307 0.03585 = 0.02343 -0.00349 0.00539 0.00378 AFIX 23 H18A 2 0.206271 0.170753 0.587635 11.00000 -1.20000 H18B 2 0.192520 0.373360 0.593238 11.00000 -1.20000 AFIX 0 C12 1 0.325510 -0.023678 0.565396 11.00000 0.03210 0.02964 = 0.02879 -0.00014 0.01349 0.00013 AFIX 43 H12 2 0.273844 -0.034816 0.566085 11.00000 -1.20000 AFIX 0 F3 5 0.191735 0.685901 0.560780 10.80000 0.14409 0.07399 = 0.05993 -0.01927 0.05571 -0.04387 C8 1 0.449314 0.552413 0.786289 11.00000 0.04329 0.04802 = 0.03035 -0.01201 0.00739 -0.00675 AFIX 137 H8A 2 0.421103 0.582152 0.809450 11.00000 -1.50000 H8B 2 0.454814 0.655344 0.767655 11.00000 -1.50000 H8C 2 0.500830 0.508234 0.804990 11.00000 -1.50000 AFIX 0 C10 1 0.305762 -0.033164 0.755027 11.00000 0.04524 0.03795 = 0.03905 0.01406 0.01857 0.00143 AFIX 137 H10A 2 0.266875 -0.000964 0.770755 11.00000 -1.50000 H10B 2 0.349274 -0.091281 0.779437 11.00000 -1.50000 H10C 2 0.282314 -0.111066 0.727077 11.00000 -1.50000 AFIX 0 C9 1 0.386757 0.251817 0.824775 11.00000 0.04309 0.05266 = 0.02286 0.00377 0.01366 0.01330 AFIX 137 H9A 2 0.355445 0.340182 0.834141 11.00000 -1.50000 H9B 2 0.441634 0.269481 0.843569 11.00000 -1.50000 H9C 2 0.370504 0.137482 0.832323 11.00000 -1.50000 AFIX 0 B1 3 0.176954 0.734584 0.605956 11.00000 0.03102 0.03050 = 0.03399 0.00374 0.00499 -0.00423 F2A 5 0.241681 0.665587 0.608134 10.20000 0.05594 F3A 5 0.154266 0.855325 0.566077 10.20000 0.03628 F4A 5 0.179718 0.851073 0.650268 10.20000 0.05323 HKLF 4 REM as500_a.res in I2/a REM wR2 = 0.1243, GooF = S = 1.081, Restrained GooF = 1.081 for all data REM R1 = 0.0458 for 3602 Fo > 4sig(Fo) and 0.0470 for all 3764 data REM 243 parameters refined using 0 restraints END WGHT 0.0599 6.7749 REM Highest difference peak 1.102, deepest hole -0.581, 1-sigma level 0.062 Q1 1 0.2244 0.7875 0.6541 11.00000 0.05 1.10 Q2 1 0.1621 0.7934 0.5559 11.00000 0.05 0.76 Q3 1 0.2320 0.6555 0.5848 11.00000 0.05 0.67 Q4 1 0.1445 0.9064 0.5719 11.00000 0.05 0.61 Q5 1 0.1536 0.8805 0.6402 11.00000 0.05 0.42 Q6 1 0.2517 0.6743 0.6250 11.00000 0.05 0.41 Q7 1 0.4505 -0.3835 0.5249 11.00000 0.05 0.39 ; _shelx_res_checksum 53278 _shelx_hkl_file ; 0 0 -2 88927.0 2499.39 46 0 0 -4 26157.3 805.156 46 0 0 -6 719024. 19991.0 46 0 0 8 348662. 9793.59 45 0 0 10 74416.5 2257.11 45 0 0 12 32301.5 1122.53 45 0 0 14 241549. 6975.90 45 0 0 16 15958.9 733.411 45 0 0 18 20.1145 86.3776 45 0 0 -18 61.5413 36.5474 7 0 0 20 5639.60 430.052 45 0 0 -20 5641.44 256.953 7 0 0 -20 6042.06 330.888 1 0 0 20 6003.23 435.307 14 0 0 22 128.422 103.210 45 0 0 -22 110.777 49.5701 7 0 0 22 146.733 98.2766 14 0 0 -24 11067.5 419.906 7 0 0 24 10277.9 654.549 45 0 0 24 9182.19 611.157 14 0 0 -26 4890.07 244.962 7 0 0 -26 5013.93 239.413 11 0 0 -28 16950.9 587.168 7 0 0 -28 17021.5 551.768 16 0 0 -28 17139.3 575.998 11 0 0 -30 14904.1 500.814 7 0 0 -30 14480.6 482.185 6 0 0 30 15579.6 501.451 12 0 0 -30 14183.1 480.538 11 0 0 -32 48.1742 25.4985 7 0 0 32 71.4139 29.6633 12 0 -1 1 1411.24 53.5719 45 0 1 1 1351.94 53.4119 45 0 -1 3 20195.6 616.865 45 0 -1 -5 10014.7 335.418 1 0 -1 5 10609.0 379.471 45 0 1 5 11120.2 381.457 45 0 -1 -7 198671. 5634.16 1 0 1 7 205247. 5702.11 45 0 -1 7 202286. 5703.82 45 0 -1 -9 46467.9 1422.11 1 0 1 9 50920.9 1508.13 45 0 -1 9 47538.7 1507.04 45 0 -1 -11 21065.0 710.721 1 0 -1 11 21415.7 798.621 45 0 1 11 21546.7 793.969 45 0 -1 -13 102985. 2948.86 1 0 1 13 100376. 3055.28 45 0 -1 13 97660.3 3053.31 45 0 -1 -15 100935. 2922.20 1 0 1 15 97559.6 3051.21 45 0 -1 15 97013.1 3053.48 45 0 -1 17 32640.1 1288.11 45 0 1 17 34217.5 1292.77 45 0 1 -17 35452.5 1049.49 7 0 -1 -17 33785.5 1044.13 7 0 1 -17 33456.7 1044.73 10 0 -1 -17 35818.8 1144.71 1 0 -1 19 22.6350 72.9912 14 0 1 19 151.615 86.3944 14 0 1 19 43.0388 86.5145 45 0 -1 19 87.3295 81.2725 45 0 1 -19 172.926 49.5262 7 0 -1 -19 210.121 51.5463 7 0 1 21 13259.4 693.287 14 0 -1 21 13278.7 737.044 14 0 1 21 13600.0 739.463 45 0 -1 21 13021.1 724.415 45 0 -1 -21 13393.2 491.234 7 0 1 -21 13955.1 497.023 7 0 -1 -21 13889.6 479.237 42 0 -1 -23 222.736 52.4292 42 0 -1 23 79.4571 90.0613 45 0 1 23 159.595 106.964 45 0 -1 23 215.731 115.906 14 0 -1 -23 167.277 48.7077 11 0 -1 -23 178.529 55.6896 7 0 1 -23 268.805 61.0150 7 0 -1 -25 45.6376 34.4459 42 0 1 25 27.4311 93.1201 45 0 -1 25 107.523 99.9599 45 0 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744.230 167.482 45 -2 2 24 609.551 160.206 45 2 -2 -24 601.726 76.1798 16 -2 -2 24 762.510 100.290 12 2 -2 -24 736.329 79.7503 11 -2 -2 24 565.445 164.633 14 2 2 -24 864.157 93.8666 7 2 -2 -24 782.946 92.6410 7 2 -2 -24 725.957 90.9657 6 2 -2 -22 1143.88 104.553 42 -2 -2 22 1146.56 200.878 45 -2 2 22 1030.91 193.215 45 2 -2 -22 999.954 95.1443 16 2 -2 -22 1110.61 98.0188 11 -2 -2 22 1156.94 213.297 14 2 2 -22 962.105 99.0535 7 2 -2 -22 1054.34 107.957 7 2 -2 -22 1335.42 114.231 6 2 -2 -20 34.8960 39.0006 42 -2 -2 20 239.671 109.702 45 -2 2 20 64.7071 76.7944 45 2 -2 -20 48.2221 38.5947 16 -2 -2 20 51.0339 94.8873 14 2 -2 -20 32.0850 31.4563 11 2 -2 -20 19.1556 40.5612 7 2 2 -20 17.1091 40.1557 7 -2 -2 18 26914.2 1125.33 14 2 -2 -18 25670.7 820.079 16 -2 -2 18 25539.6 1053.44 45 -2 2 18 25744.5 1049.02 45 2 -2 -18 26472.0 837.970 7 2 2 -18 26415.2 826.348 7 2 -2 -18 26459.1 831.690 42 -2 -2 16 3203.57 301.117 14 -2 2 16 3251.32 236.494 14 -2 2 16 3175.77 270.033 45 -2 -2 16 3212.08 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714.352 101.881 45 2 -2 10 19429.5 713.656 45 2 2 10 19853.4 713.000 45 2 -2 12 29.7633 61.9138 45 2 2 12 188.348 82.3277 45 2 2 14 2548.90 249.058 45 2 -2 14 2918.86 267.090 45 2 -2 16 207.766 97.2230 45 2 2 16 99.9384 83.1084 45 -2 -2 -16 18.9859 29.7473 7 -2 -2 -16 55.8270 33.1724 10 -2 2 -16 79.7874 35.5390 10 -2 -2 -18 39120.3 1203.22 7 -2 2 -18 38835.4 1207.49 10 -2 2 -18 40917.2 1222.01 7 2 -2 18 40559.7 1527.58 45 2 2 18 40122.2 1511.42 45 2 2 20 2188.54 273.821 45 2 -2 20 1280.09 223.825 45 2 -2 20 1916.83 272.449 14 -2 -2 -20 1967.03 137.162 16 -2 2 -20 1846.95 136.841 7 -2 -2 -20 1705.21 124.472 7 -2 -2 -20 1853.08 125.877 19 -2 -2 -22 1903.64 127.856 6 -2 -2 -22 2452.32 155.849 42 2 2 22 1864.84 259.875 45 2 -2 22 1903.68 266.987 45 2 -2 22 2354.36 307.370 14 -2 -2 -22 2385.89 152.544 16 -2 -2 -22 2245.97 141.514 7 -2 2 -22 2205.02 151.348 7 -2 -2 -22 2186.12 138.992 19 -2 -2 -24 32242.3 981.159 19 -2 -2 -24 32180.0 999.924 16 -2 -2 -24 34005.1 1004.01 42 -2 2 -24 33600.1 1013.44 7 -2 -2 -24 30001.2 982.547 7 -2 -2 -24 29789.0 964.620 6 2 -2 26 22995.2 742.941 12 -2 -2 -26 22631.8 727.506 16 -2 -2 -26 23539.7 725.849 42 -2 -2 -26 21522.9 712.828 7 -2 2 -26 23668.8 745.004 7 -2 -2 -26 21894.2 702.174 19 -2 -2 -28 43.9825 30.1827 42 2 -2 28 50.2695 41.3456 12 -2 -2 -28 31.1621 32.6711 16 -2 2 -28 31.6084 42.5432 7 -2 2 -28 22.8606 34.3683 11 2 -2 30-8.97644 25.2923 12 2 2 30 21.7206 26.8718 12 -2 2 -30 17.5813 27.0596 11 -2 2 -30 30.5457 31.2799 7 2 -3 -31 5821.70 217.397 35 2 3 -31 6453.92 227.790 11 2 3 -31 5815.22 213.612 7 -2 -3 29 13930.9 468.140 33 2 3 -29 15626.5 493.506 7 2 3 -29 15763.6 506.940 11 -2 -3 29 14780.3 502.988 12 -2 -3 27 38629.7 1207.70 12 2 3 -27 39374.1 1203.39 11 2 -3 -27 37339.3 1175.12 6 2 3 -27 40144.3 1190.21 7 2 -3 -27 38836.9 1182.47 7 2 -3 -27 41563.9 1196.77 42 -2 -3 25 9995.64 405.046 12 2 -3 -25 10349.0 386.174 6 2 -3 -25 9964.60 386.270 7 2 3 -25 10041.3 383.138 7 2 -3 -25 9889.02 389.025 42 2 -3 -23 218.523 65.0025 42 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30177.3 913.722 7 2 -3 -17 29376.8 930.299 7 2 -3 -17 27154.4 908.131 19 2 -3 -15 18055.2 578.363 42 -2 -3 15 16702.5 553.545 39 2 -3 -15 16528.4 564.091 16 -2 -3 15 16374.3 578.631 12 -2 -3 15 17636.4 823.742 14 -2 3 15 16742.8 711.941 45 -2 -3 15 17551.7 729.893 45 -2 -3 13 108967. 3417.75 14 -2 3 13 109441. 3289.13 45 -2 -3 13 111163. 3300.36 45 -2 -3 11 22628.0 917.967 14 -2 3 11 23237.1 831.088 45 -2 -3 11 23219.7 835.054 45 -2 -3 9 8022.37 422.569 14 -2 -3 9 8442.68 369.973 45 -2 3 9 8547.43 369.251 45 -2 -3 7 14061.8 561.820 14 -2 3 7 13656.2 484.229 45 -2 -3 7 12903.5 479.386 45 -2 -3 5 311616. 7874.26 18 -2 -3 5 280340. 7826.29 14 -2 3 5 282717. 7719.08 13 2 -3 -5 301236. 7852.35 18 -2 -3 3 34735.3 1195.02 18 2 -3 -3 38951.3 1196.79 18 2 -3 -1 7563.94 246.928 14 -2 -3 1 8907.31 371.851 18 2 -3 -1 8251.66 367.677 18 -2 -3 -1 27876.6 937.368 18 2 -3 3 930.045 71.2999 45 2 3 3 891.341 66.8341 45 2 -3 5 25269.7 813.559 45 2 3 5 25008.5 806.913 45 2 -3 7 25819.9 872.732 45 2 3 7 25690.5 869.311 45 2 -3 9 5285.81 304.522 45 2 3 9 5534.05 309.269 45 2 -3 11 50609.2 1702.31 45 2 3 11 53306.1 1713.27 45 -2 -3 -13 85.4406 41.6189 16 2 3 13 166.288 75.8113 45 2 -3 13 185.067 70.0327 45 -2 -3 -13 142.831 46.9585 19 2 -3 15 84.6341 33.4915 38 2 3 15 57.2635 61.6093 45 2 -3 15 196.166 94.2609 45 -2 -3 -15 211.231 57.2263 16 -2 3 -15 153.062 38.6488 10 -2 -3 -17 9152.54 368.595 16 2 -3 17 8505.20 573.441 14 2 3 17 9132.39 541.024 45 2 -3 17 8788.67 538.925 45 -2 -3 -17 9586.23 360.739 19 2 -3 17 8183.58 314.074 38 2 -3 19 11473.7 677.127 45 2 3 19 12039.6 675.027 45 2 -3 19 12499.5 747.032 14 -2 -3 -19 13428.3 494.862 16 -2 3 -19 13488.7 479.785 7 -2 -3 -19 13309.2 479.707 19 -2 -3 -21 3675.41 201.480 42 2 -3 21 3433.67 176.077 39 2 -3 21 3161.79 329.284 45 2 -3 21 2920.18 344.697 14 -2 -3 -21 3710.18 204.924 16 -2 -3 -21 3549.52 189.845 19 -2 3 -21 3375.85 190.754 7 -2 -3 -23 13977.6 508.746 16 2 -3 23 14104.0 512.540 12 -2 -3 -23 15149.6 517.863 42 2 -3 23 13501.7 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22 -7 -4 -17 18890.3 667.066 16 7 -4 17 19287.4 620.577 38 -7 -4 -17 18947.3 615.689 22 -7 -4 -17 20213.3 668.967 19 -7 -4 -19 17.5144 44.7560 16 -7 4 -19 71.6959 45.3328 7 7 -4 19 6.53043 27.6024 38 7 -4 19 32.7018 40.7421 39 -7 -4 -19-5.59245 48.0265 19 -7 -4 -21 820.550 78.9335 42 7 -4 21 935.972 72.6436 39 -7 4 -21 681.195 70.4894 7 -7 -4 -21 817.867 76.8758 19 -7 4 -23 2181.46 108.947 7 7 -4 23 2181.22 94.8021 39 -7 4 -25 3393.17 124.938 11 7 -5 -28 17.7179 23.8484 35 -7 -5 28 6.15147 29.5356 34 7 -5 -28 30.1422 17.5299 26 7 -5 -26 6104.68 233.340 35 -7 -5 26 6091.28 243.095 34 7 -5 -24 10296.0 386.676 35 -7 -5 24 10480.1 399.599 34 7 -5 -22 3611.51 200.380 35 -7 -5 22 3605.94 168.747 33 7 -5 -22 3989.24 213.691 6 7 -5 -20 9543.19 382.381 35 -7 -5 20 9240.11 345.878 33 7 -5 -20 9194.77 356.823 40 7 -5 -20 8856.57 385.115 6 7 -5 -18 6252.39 291.684 35 -7 -5 18 6349.97 265.066 33 7 -5 -18 5799.24 271.115 40 7 -5 -18 5959.59 293.248 6 7 -5 -16 14.0035 32.0829 20 7 -5 -16-6.61876 42.0315 40 -7 -5 16 11.2978 42.0095 33 7 -5 -16-28.8067 56.8060 35 -7 -5 16-7.63823 56.8039 34 7 -5 -16 8.05973 25.9542 30 7 -5 -16-38.6729 51.8481 6 7 -5 -14 2856.69 180.846 35 -7 -5 14 2863.21 145.832 31 -7 -5 14 3178.23 190.191 34 -7 -5 14 3358.50 173.075 33 -7 -5 14 3253.50 156.847 17 7 -5 -14 2677.66 170.770 40 7 -5 -14 3061.93 159.979 20 7 -5 -12 5573.28 266.230 40 -7 -5 12 6308.76 248.719 17 7 -5 -12 6398.62 282.156 35 -7 -5 12 6526.87 282.986 34 -7 -5 12 6134.22 243.674 31 7 -5 -12 5791.94 260.138 26 7 -5 -12 5906.47 251.598 20 7 -5 -10 59904.9 1818.27 40 7 -5 -10 58771.5 1785.70 37 -7 -5 10 65659.9 1798.00 17 -7 -5 10 62493.4 1824.74 34 -7 -5 10 61523.0 1789.84 31 7 -5 -10 63820.6 1831.31 35 7 -5 -10 59559.8 1776.42 29 7 -5 -10 58906.5 1805.27 26 7 -5 -10 65282.3 1805.27 20 -7 -5 10 60840.8 2020.43 18 7 -5 -8 1081.70 97.4493 40 7 -5 -8 1218.38 98.0349 37 -7 -5 8 1080.99 158.889 18 -7 -5 8 1305.72 93.6649 17 -7 -5 8 1215.70 105.070 34 -7 -5 8 1137.88 87.6371 31 7 -5 -8 1271.77 106.397 35 7 -5 -8 1180.34 95.8301 26 7 -5 -8 1187.22 90.0583 29 7 -5 -8 1169.07 92.7472 20 7 -5 -6 38859.1 1212.47 40 -7 -5 6 39982.2 1190.20 17 -7 -5 6 40933.6 1191.63 31 -7 -5 6 40206.7 1215.34 34 7 -5 -6 41103.3 1219.54 35 7 -5 -6 39802.5 1201.63 26 7 -5 -6 40621.9 1208.31 29 -7 -5 6 42515.7 1422.06 18 7 -5 -6 42411.0 1205.24 20 -7 -5 6 37131.7 1183.91 22 7 -5 -6 38903.2 1203.18 25 7 -5 -4 50450.3 1530.71 38 -7 -5 4 48206.6 1537.54 41 7 -5 -4 51467.3 1550.67 40 -7 -5 4 51971.1 1521.69 17 7 -5 -4 53090.2 1558.64 29 7 -5 -4 50322.1 1542.95 27 7 -5 -4 51102.4 1534.28 25 7 -5 -4 51366.4 1545.78 28 7 -5 -4 51273.3 1532.26 26 7 -5 -4 57140.1 1543.64 20 7 -5 -4 59435.5 1809.32 18 -7 -5 4 51496.7 1534.66 22 -7 -5 4 53001.0 1525.60 31 -7 -5 4 55205.0 1555.44 34 7 -5 -4 53231.0 1550.97 35 -7 -5 2 25756.5 838.682 41 7 -5 -2 27761.5 830.004 25 7 -5 -2 26876.8 840.851 27 7 -5 -2 26207.9 858.062 29 7 -5 -2 26304.9 839.394 28 -7 -5 2 25995.8 816.682 23 -7 -5 2 25414.3 838.011 22 7 -5 -2 26672.3 1047.07 18 -7 -5 2 28651.9 825.306 31 7 -5 -2 27630.3 846.961 35 -7 -5 0 116564. 3394.70 41 7 -5 0 115957. 3399.74 30 7 -5 0 117897. 3389.45 27 7 -5 0 119713. 3373.64 25 7 -5 0 120416. 3393.23 28 -7 -5 0 119719. 3371.62 23 -7 -5 0 115154. 3405.53 22 7 -5 0 115985. 3640.60 18 -7 -5 0 125583. 3376.15 31 7 -5 2 11509.2 423.401 37 -7 -5 -2 11514.8 404.770 41 7 -5 2 11071.5 393.361 27 7 -5 2 10721.5 418.174 29 7 -5 2 11006.8 394.060 28 7 -5 2 11273.9 403.646 30 -7 -5 -2 11002.4 379.002 23 -7 -5 -2 9776.06 406.794 22 7 -5 2 9973.82 564.788 18 -7 -5 -2 10900.6 379.216 36 7 -5 2 10718.4 385.677 33 7 -5 4 2376.74 149.097 37 -7 -5 -4 1940.94 131.437 41 7 -5 4 2361.80 149.946 29 -7 -5 -4 2014.05 121.496 26 7 -5 4 2263.58 131.807 27 7 -5 4 1949.72 124.822 28 7 -5 4 2031.78 130.363 30 7 -5 4 1780.68 226.723 18 -7 -5 -4 1966.18 137.827 19 -7 -5 -4 2090.85 118.935 23 -7 -5 -4 2040.52 118.018 36 7 -5 4 2060.76 130.464 33 7 -5 6 11275.0 421.766 37 -7 -5 -6 10990.4 388.932 36 7 -5 6 11985.7 431.172 29 7 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1938.28 109.711 33 -7 -5 -20 2010.94 111.499 42 7 -5 20 2136.98 108.473 39 -7 5 -20 2120.88 107.136 7 7 -5 22 466.710 41.6875 33 7 -5 22 474.631 37.3886 39 -7 -5 -22 546.753 46.1558 42 -7 5 -22 455.825 38.2526 7 7 -6 -27 548.494 38.6417 27 -7 -6 27 713.388 46.5548 34 7 -6 -25 381.998 37.5285 26 7 -6 -25 470.247 50.4157 35 7 -6 -23 142.233 37.2428 26 7 -6 -23 133.927 43.4020 35 -7 -6 23 105.611 45.0461 34 7 -6 -21 85.3754 40.4149 26 7 -6 -21 81.8350 49.3942 35 -7 -6 21 69.2471 51.1263 34 7 -6 -19 122.644 41.2727 28 7 -6 -19 137.125 48.8159 26 7 -6 -19 100.151 53.0122 35 -7 -6 19 125.916 60.0352 34 7 -6 -17 97.6371 45.4463 26 7 -6 -17 157.603 56.5060 28 7 -6 -17 109.358 38.0729 20 7 -6 -17 188.548 41.2383 24 7 -6 -17 141.383 61.0003 35 -7 -6 17 98.7910 57.2997 34 -7 -6 17 124.619 33.7484 31 7 -6 -15 70.8549 40.5465 40 7 -6 -15 30.2439 28.9985 30 7 -6 -15 41.6388 46.9317 26 7 -6 -15 26.1556 49.6420 28 7 -6 -15-4.65872 33.1871 20 -7 -6 15 81.1862 34.7746 31 7 -6 -15 27.3863 55.9791 35 -7 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1446.76 115.339 35 7 -6 -7 1483.36 123.988 30 7 -6 -7 1520.11 114.343 25 7 -6 -7 1431.76 104.803 29 7 -6 -7 1278.50 113.607 27 7 -6 -7 1595.47 114.677 26 7 -6 -7 1667.37 115.569 20 7 -6 -5 5030.69 236.949 37 -7 -6 5 4575.78 219.922 41 7 -6 -5 4449.49 199.712 38 -7 -6 5 5230.35 218.638 17 7 -6 -5 5073.00 246.055 30 7 -6 -5 4903.54 223.820 25 7 -6 -5 5097.24 230.299 29 7 -6 -5 4681.06 227.852 27 7 -6 -5 4636.36 229.465 28 7 -6 -5 5001.12 221.692 26 -7 -6 5 4731.82 212.293 22 -7 -6 5 4915.46 215.109 31 7 -6 -5 4762.92 203.392 31 7 -6 -3 258.970 53.4248 38 7 -6 -3 293.794 63.9350 37 -7 -6 3 236.184 56.3415 41 7 -6 -3 206.090 55.4481 28 7 -6 -3 294.074 62.9451 29 7 -6 -3 245.615 60.9572 27 -7 -6 3 272.841 53.1014 23 -7 -6 3 245.594 52.7224 22 -7 -6 3 288.379 46.1035 20 7 -6 -3 268.764 53.1245 25 -7 -6 3 303.486 53.2037 31 -7 -6 1 5030.42 227.978 41 7 -6 -1 4830.39 247.594 37 7 -6 -1 4936.36 233.358 38 -7 -6 1 5196.72 219.880 31 7 -6 -1 4985.79 217.105 25 7 -6 -1 5018.49 230.141 27 7 -6 -1 5009.62 248.989 29 7 -6 -1 4809.72 229.352 28 7 -6 -1 5437.43 250.666 30 -7 -6 1 4952.07 215.037 23 7 -6 -1 4897.62 378.804 18 -7 -6 1 4759.10 232.711 22 7 -6 1 1476.68 112.440 39 -7 -6 -1 1627.92 115.847 41 7 -6 1 1426.23 122.211 38 7 -6 1 1346.91 202.242 18 7 -6 1 1451.74 101.024 33 -7 -6 -1 1533.06 107.795 36 7 -6 1 1485.29 111.611 27 7 -6 1 1582.04 115.445 28 7 -6 1 1515.93 123.821 30 -7 -6 -1 1759.52 110.608 23 -7 -6 -1 1686.80 131.432 22 7 -6 3 94.0857 56.4864 37 7 -6 3 125.853 59.2336 38 7 -6 3 123.486 56.3821 39 7 -6 3 172.262 89.6095 18 7 -6 3 228.732 60.8986 30 7 -6 3 160.332 63.6214 29 7 -6 3 163.480 54.7130 27 -7 -6 -3 117.236 36.9219 26 -7 -6 -3 177.430 49.8392 23 -7 -6 -3 133.760 61.9876 22 7 -6 3 189.721 43.9829 33 -7 -6 -3 114.847 47.8228 36 7 -6 5 3738.12 203.611 39 7 -6 5 3726.40 209.998 38 7 -6 5 3575.51 197.500 37 -7 -6 -5 3268.25 170.057 26 7 -6 5 4172.45 212.098 29 7 -6 5 3647.13 188.065 30 7 -6 5 3086.68 314.889 18 7 -6 5 3519.30 170.833 24 -7 -6 -5 4250.79 184.985 23 -7 -6 -5 3821.37 176.727 36 7 -6 5 3457.23 181.179 33 7 -6 7-13.7693 50.1227 39 7 -6 7 40.3213 48.2920 37 7 -6 7-9.83856 45.7306 30 -7 -6 -7-4.88545 33.9870 26 7 -6 7 102.423 56.3800 29 -7 -6 -7 21.0323 55.3011 22 7 -6 7-11.4370 37.8401 33 -7 -6 -7 28.8375 37.2622 36 -7 -6 -9 2729.25 161.052 42 7 -6 9 3325.64 188.535 39 7 -6 9 3100.72 165.381 37 7 -6 9 3108.34 181.872 38 7 -6 9 3236.67 171.929 29 -7 -6 -9 2961.59 158.649 26 7 -6 9 3414.35 159.579 30 -7 -6 -9 3166.91 184.320 22 7 -6 9 2852.59 170.364 33 -7 -6 -11 1778.95 120.379 42 7 -6 11 1611.98 127.033 39 7 -6 11 1667.37 109.777 37 7 -6 11 1742.48 125.126 38 -7 -6 -11 1497.45 107.104 26 7 -6 11 1799.53 100.596 30 7 -6 11 1652.83 122.382 33 -7 -6 -11 1687.38 123.706 22 7 -6 13 876.742 88.5488 33 -7 -6 -13 1010.39 88.7499 22 -7 -6 -13 880.706 84.6338 42 7 -6 13 926.956 92.0579 39 7 -6 13 932.036 85.4837 38 7 -6 15 12870.4 412.178 32 7 -6 15 14119.3 459.774 33 7 -6 15 12394.2 408.604 17 -7 6 -15 14285.9 440.275 7 7 -6 15 14394.5 448.647 38 -7 -6 -15 13977.0 452.567 42 7 -6 17 416.002 50.5387 33 7 -6 17 525.981 55.4788 39 -7 -6 -17 493.215 51.1448 42 -7 -6 -17 475.417 41.7516 21 -7 6 -17 452.282 43.7193 7 7 -6 19 2285.15 96.2227 31 7 -6 19 2334.14 101.518 33 7 -7 -22 7768.88 254.139 27 7 -7 -22 8482.63 264.246 25 7 -7 -22 8193.57 260.162 35 7 -7 -20 13872.9 466.419 27 7 -7 -20 14932.2 475.521 25 7 -7 -20 13706.6 449.203 26 -7 -7 20 14803.7 476.095 34 7 -7 -20 14502.1 470.098 35 7 -7 -18 2320.34 137.232 25 7 -7 -18 2148.59 130.129 27 7 -7 -18 2183.07 117.828 26 -7 -7 18 2074.71 132.866 34 7 -7 -18 2281.64 133.906 35 7 -7 -16 3406.19 181.919 25 7 -7 -16 3436.42 180.099 27 7 -7 -16 3623.46 166.360 28 7 -7 -16 3624.57 169.544 26 7 -7 -16 3266.86 146.420 24 -7 -7 16 3430.29 139.743 31 -7 -7 16 3868.86 193.099 34 7 -7 -16 3421.75 178.575 35 -7 -7 14 3537.59 168.780 41 7 -7 -14 3347.95 182.532 27 7 -7 -14 3448.19 177.410 28 7 -7 -14 3760.75 191.402 25 7 -7 -14 3493.71 172.863 26 7 -7 -14 3441.78 164.010 24 -7 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8 -7 -9 3496.85 184.172 27 8 -7 -9 3541.26 189.451 28 8 -7 -9 3482.79 174.967 25 8 -7 -9 3893.42 193.489 30 -8 -7 9 3440.50 166.233 23 8 -7 -9 3331.76 150.937 32 -8 -7 9 3900.81 174.160 31 -8 -7 7 78.5075 45.6393 41 8 -7 -7 36.6651 36.1848 37 8 -7 -7 80.7605 54.1965 30 8 -7 -7 46.5652 47.4765 27 -8 -7 7 81.2693 40.7135 23 8 -7 -7 59.1009 39.6754 25 -8 -7 7 50.6035 40.0074 31 8 -7 -7 44.0880 32.5184 32 -8 -7 5 78.0682 43.5252 41 8 -7 -5 27.2496 46.8183 37 8 -7 -5 12.7083 49.6719 30 8 -7 -5 100.088 50.1217 27 8 -7 -5 96.7516 55.0547 28 -8 -7 5 29.6955 32.3962 21 -8 -7 5 36.6557 39.6104 23 8 -7 -5 43.3493 35.4617 25 -8 -7 3 91.7370 46.1004 41 8 -7 -3 54.6844 48.4029 37 8 -7 -3 53.1451 46.9965 27 8 -7 -3 44.9233 30.6571 31 8 -7 -3 98.8428 51.5150 28 -8 -7 3 123.205 44.7798 23 -8 -7 3 37.2100 37.4387 36 8 -7 -1 1996.02 123.757 38 8 -7 -1 2082.02 144.608 37 8 -7 -1 1973.85 126.092 27 8 -7 -1 2119.57 142.309 29 8 -7 -1 2155.33 142.082 30 8 -7 -1 1906.72 129.714 24 -8 -7 1 1930.18 114.196 23 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13-4.04051 14.2393 32 -8 -7 -15 2929.23 110.420 20 8 -7 15 2730.49 106.782 31 8 -8 -16 3111.68 127.993 25 8 -8 -16 3193.09 128.999 27 8 -8 -14 2091.36 102.634 25 8 -8 -14 1995.30 103.741 27 -8 -8 14 1982.07 87.9529 23 8 -8 -14 2093.31 92.2193 24 8 -8 -12 16624.0 551.271 27 -8 -8 12 17210.6 534.053 23 -8 -8 10 7047.16 248.150 23 8 -8 -10 7251.05 266.920 24 8 -8 -8 1101.73 80.8017 30 -8 -8 8 1044.31 70.0663 23 -8 -8 8 968.940 73.2655 36 8 -8 -6 18145.4 595.233 30 8 -8 -6 19149.0 604.413 24 -8 -8 6 19122.4 574.224 23 -8 -8 6 18031.8 576.604 36 8 -8 -4 760.656 77.6715 30 8 -8 -4 994.618 83.6475 24 -8 -8 4 905.756 67.2565 23 8 -8 -4 829.356 67.3787 32 -8 -8 4 833.576 68.0827 36 8 -8 -2 539.506 62.3689 24 -8 -8 2 495.521 49.7317 21 -8 -8 2 510.237 52.8697 23 8 -8 -2 539.417 58.6245 32 -8 -8 2 523.054 52.8547 36 8 -8 0 1529.29 97.5744 30 8 -8 0 1317.45 84.0536 24 -8 -8 0 1365.36 85.9351 21 8 -8 0 1335.99 92.1653 32 -8 -8 0 1416.83 81.4769 36 -8 -8 -2 1564.00 83.0221 36 8 -8 2 1524.34 85.3679 31 8 -8 2 1469.53 78.3499 24 -8 -8 -2 1407.74 89.6886 21 8 -8 2 1494.62 91.5563 30 8 -8 4 9722.13 328.680 31 8 -8 4 10174.2 337.199 32 8 -8 4 10159.8 329.123 30 -8 -8 -4 9450.06 334.951 21 8 -8 6 807.894 53.0977 30 8 -8 6 782.747 58.8224 32 8 -8 6 749.648 56.4250 17 8 -8 8 430.554 40.4879 31 8 -8 8 558.215 41.5726 32 -8 -8 -8 569.622 47.3697 21 8 -8 8 463.341 38.5674 17 -8 -8 -10 7058.35 209.993 21 8 -8 10 6004.86 205.741 31 -9 0 35-3.96137 15.9105 8 9 0 -33-25.1960 33.0135 7 9 0 -33-3.29741 28.5389 6 9 0 -31 56.6399 47.5473 7 9 0 -31 23.3180 39.4189 6 -9 0 31-3.56600 29.8985 2 9 0 -29-6.47468 51.0810 7 -9 0 29-44.0902 37.1963 2 9 0 -29-40.6780 47.5151 6 9 0 -27 51.9640 58.0131 7 9 0 -27 22.1289 55.9899 11 9 0 -27 26.3406 49.9852 6 -9 0 27 5.36028 37.2927 12 -9 0 25-30.3501 92.1449 45 9 0 -25 15.7771 61.6459 47 9 0 -25 15.7815 56.1840 7 9 0 -25 27.7506 48.2622 6 -9 0 25 5.90682 40.1012 12 9 0 -23-30.1576 91.5620 46 9 0 -23 15.4266 65.7195 47 9 0 -23 235.975 67.0189 7 9 0 -23-20.5847 49.4114 6 9 0 -23 21.9259 74.4279 1 -9 0 23 5.97025 40.0257 12 9 0 -21 28.2445 85.7521 46 9 0 -21 7.12316 50.7191 47 9 0 -21-22.0942 49.3698 7 9 0 -21-64.1314 85.8578 1 9 0 -21-25.7396 40.2771 6 -9 0 21 28.3797 39.0129 12 9 0 -19 124.462 80.1659 46 9 0 -19 18.8640 50.0672 47 9 0 -19 33.4889 46.6048 7 9 0 -19 63.7639 45.7360 6 -9 0 19 20.5403 33.9948 12 9 0 -17 107.928 89.7384 46 9 0 -17 36.1861 75.2194 1 9 0 -17-10.0973 30.1770 6 9 0 -17 6.14982 36.1598 11 9 0 -17 58.7362 40.3732 7 9 0 -15 111.513 79.8013 46 9 0 -15 48.0659 76.9146 1 9 0 -15 5.40466 30.7041 11 9 0 -13-41.9586 63.7004 1 9 0 -13-16.3153 60.6729 46 -9 0 11 96.3881 68.9767 13 9 0 -11 14.8916 69.6770 46 9 0 -11-24.0265 53.1693 1 -9 0 9-14.5511 60.4932 13 9 0 -9-13.8113 64.6214 46 9 0 -9-11.3455 50.2126 43 9 0 -9 92.5917 57.3821 1 -9 0 7 28.5842 63.2535 13 9 0 -7-11.2568 49.8200 43 -9 0 5 42.3440 62.4708 13 9 0 -5 32.6996 32.1654 44 9 0 -5-11.2816 55.4968 43 9 0 -3 11.4800 52.2810 43 9 0 -3 3.67091 28.6868 44 9 0 -1 38.2218 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3912.26 43 9 -2 1 133275. 3669.54 44 9 2 1 130864. 3663.85 44 9 -2 3 13497.8 633.881 43 9 -2 3 13674.5 461.048 44 9 2 3 12806.8 451.580 44 9 -2 3 13471.4 646.580 45 9 2 3 13298.6 635.899 45 9 -2 5 31458.4 1173.42 43 -9 2 -5 31759.9 958.433 10 -9 -2 -5 31329.1 959.735 5 -9 -2 -5 30452.3 953.684 4 -9 2 -5 31680.9 946.586 4 9 -2 5 29414.3 958.205 44 9 2 5 31123.4 960.060 44 9 -2 5 28812.7 1193.39 45 9 2 5 30721.9 1200.02 45 9 -2 7 7020.60 443.219 43 -9 2 -7 7505.95 311.521 10 -9 -2 -7 7861.07 316.880 10 -9 2 -7 7662.98 301.314 4 -9 -2 -7 8270.43 321.987 5 9 2 7 7895.98 507.203 45 9 -2 7 7972.38 516.982 45 9 -2 9 7627.30 454.346 43 9 2 9 7509.55 525.770 45 9 -2 9 8866.50 569.122 45 -9 2 -9 7812.72 326.171 10 -9 -2 -9 7732.16 326.514 10 -9 2 -9 8112.54 314.543 4 -9 -2 -11 3928.87 207.228 10 -9 2 -11 3689.08 202.158 10 9 2 11 3449.76 362.451 45 9 -2 11 3594.75 370.959 45 9 -2 11 3972.47 189.619 15 -9 2 -13 3396.98 192.084 10 -9 -2 -13 3342.20 191.875 10 9 2 13 2848.33 345.689 45 9 -2 13 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1 0 295.951 55.0885 44 11 -1 2 21315.0 940.180 43 -11 1 -2 22505.7 728.295 9 -11 1 -2 23771.0 736.514 4 -11 -1 -2 22982.1 734.659 4 11 -1 2 22560.4 742.204 44 11 1 2 22528.9 738.222 44 11 -1 4 1168.21 184.817 43 -11 -1 -4 695.674 82.2214 10 -11 1 -4 763.234 79.2441 9 -11 1 -4 804.948 86.2645 10 -11 -1 -4 916.631 88.6294 4 -11 1 -4 723.276 79.1395 4 11 -1 4 966.965 182.176 45 11 1 4 864.466 175.823 45 11 -1 4 1062.65 98.4547 44 11 1 4 711.433 86.2387 44 11 -1 6 38397.3 1466.18 43 -11 1 -6 39560.3 1225.04 10 -11 -1 -6 39501.5 1229.09 10 -11 1 -6 39038.1 1202.42 5 -11 -1 -6 39882.6 1221.30 5 -11 -1 -6 40842.2 1228.24 4 -11 1 -6 40486.8 1220.19 4 11 -1 6 39611.3 1239.54 44 11 1 6 39369.6 1234.63 44 11 -1 6 37513.7 1540.69 45 11 1 6 40937.3 1563.48 45 11 -1 8 46783.6 1828.27 43 -11 -1 -8 52645.3 1608.17 10 -11 1 -8 52191.6 1603.14 10 -11 1 -8 52812.2 1578.82 5 -11 -1 -8 55562.0 1603.26 5 -11 1 -8 55207.7 1600.01 4 11 -1 8 52755.7 1623.72 44 11 1 8 54176.4 1623.08 44 11 -1 8 49449.2 1967.96 45 11 1 8 49566.5 1956.75 45 11 -1 10 81.6003 65.7466 43 -11 -1 -10 126.270 54.7241 10 -11 1 -10 115.228 52.4978 10 -11 1 -10 149.105 48.9325 5 -11 -1 -10 100.648 55.3870 5 -11 1 -10 91.5731 48.2077 4 11 -1 10 31.3648 121.418 45 11 1 10 92.1375 114.232 45 11 -1 10 49.7539 58.4286 44 11 1 10 89.2647 65.8179 44 11 -1 12 4670.51 255.314 44 11 1 12 4497.91 249.181 44 11 -1 12 4082.50 432.314 45 11 1 12 4093.41 428.225 45 -11 -1 -12 4725.57 242.876 10 -11 1 -12 4471.27 238.064 10 11 -1 12 4231.18 339.521 43 -11 -1 -14 6086.79 279.358 10 -11 1 -14 6009.96 278.011 10 11 -1 14 5813.18 243.886 15 11 -1 14 5512.81 286.530 44 11 1 14 5725.67 287.210 44 11 -1 16 29598.8 891.244 15 11 -1 16 27689.7 943.851 44 11 1 16 29203.9 947.458 44 -11 1 -16 29735.9 916.684 7 -11 -1 -16 29042.5 932.033 10 -11 1 -16 28613.3 927.714 10 -11 -1 -16 29380.9 880.135 22 -11 -1 -18 23.1063 35.4391 16 11 -1 18 32.7147 27.8906 15 11 -1 18 30.1056 45.2527 44 11 1 18 58.4426 43.9242 44 -11 -1 -18 5.26614 44.8781 10 -11 1 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47 11 -2 -23 3047.96 202.197 7 11 2 -23 3182.70 176.417 7 11 2 -23 3366.28 322.742 1 11 -2 -23 2877.53 188.125 6 -11 -2 23 3295.37 186.420 2 -11 2 23 3130.02 359.668 13 -11 -2 23 2551.76 325.039 13 11 -2 -21 6245.53 508.699 46 11 2 -21 5354.88 471.118 46 11 -2 -21 6248.66 292.009 47 11 2 -21 6047.75 286.895 47 11 -2 -21 6403.36 309.588 7 11 2 -21 5677.40 435.733 1 -11 -2 21 6307.35 289.258 2 11 -2 -21 6343.34 293.601 6 -11 2 21 5575.01 482.667 13 -11 -2 21 5215.78 472.811 13 11 -2 -19 49162.1 1850.09 46 11 2 -19 48574.1 1825.09 46 11 -2 -19 49114.7 1484.04 47 11 2 -19 49424.5 1477.19 47 11 -2 -19 49383.7 1504.52 7 11 2 -19 48155.0 1742.73 1 -11 -2 19 48601.0 1484.79 2 11 -2 -19 49096.0 1481.71 6 -11 2 19 43843.5 1803.80 13 11 -2 -17 3083.89 331.770 46 11 2 -17 2665.98 308.292 46 -11 -2 17 3572.46 195.982 2 11 2 -17 3763.33 321.559 1 11 -2 -17 3121.05 181.989 6 -11 2 17 2452.19 296.334 13 -11 -2 17 3180.10 334.875 13 11 -2 -15 80734.1 2654.87 46 11 2 -15 78525.7 2632.25 46 -11 -2 15 80667.6 2340.71 8 11 2 -15 79292.2 2562.86 1 -11 -2 15 81812.0 2335.36 2 11 -2 -15 77558.6 2317.22 6 -11 2 15 80065.4 2658.73 13 -11 -2 15 76772.4 2646.47 13 11 -2 -13 44667.7 1587.11 46 11 2 -13 43209.8 1559.87 46 -11 2 13 42698.6 1578.33 13 -11 -2 13 41367.3 1575.43 13 -11 2 13 41449.2 1293.89 8 -11 -2 13 43111.6 1313.58 8 11 2 -13 44405.5 1498.29 1 -11 -2 13 42500.0 1305.27 2 11 -2 -13 44259.3 1296.78 6 11 2 -11 5303.09 323.078 43 11 -2 -11 5501.74 402.533 46 11 2 -11 6027.87 410.512 46 -11 2 11 5860.22 417.865 13 -11 -2 11 5995.24 424.932 13 -11 -2 11 6001.27 262.793 8 -11 2 11 5859.57 249.573 8 -11 -2 11 6161.42 263.294 3 11 2 -11 6119.69 356.960 1 11 -2 -11 6397.72 253.245 6 -11 -2 11 5750.13 252.565 2 -11 2 11 5682.74 239.792 2 11 2 -9 59817.5 1823.26 43 -11 -2 9 55344.3 1659.05 8 -11 -2 9 54379.5 1656.95 3 11 2 -9 54733.5 1770.77 1 11 -2 -9 57445.6 1642.21 6 11 -2 -9 55480.8 1911.19 46 11 2 -9 55093.4 1888.72 46 -11 -2 7 72488.5 2087.84 2 -11 -2 7 70727.0 2094.33 3 11 2 -7 73281.5 2278.20 43 -11 -2 7 72044.4 2098.38 8 -11 -2 5 57135.6 1684.74 3 11 2 -5 56123.7 1862.37 43 11 -2 -5 57351.8 1671.30 40 11 -2 -3 1097.48 84.9312 15 11 2 -3 1311.95 96.5978 44 11 -2 -3 1175.51 95.4396 44 -11 -2 3 1210.63 97.8138 9 -11 -2 3 1072.29 81.5252 41 11 -2 -3 1123.30 87.8083 40 11 -2 -3 980.838 169.190 43 -11 -2 1 25079.0 788.090 41 11 -2 -1 27051.5 807.449 40 11 -2 -1 26404.4 1058.03 43 11 -2 -1 26685.9 821.872 44 11 2 -1 25345.4 811.052 44 11 -2 -1 26313.7 806.459 15 -11 2 1 25742.2 803.165 9 -11 -2 1 25365.0 816.928 9 -11 -2 1 25062.8 803.507 4 -11 -2 -1 28491.7 864.191 41 11 -2 1 29680.7 1158.35 43 11 -2 1 28012.7 898.082 44 11 2 1 28494.5 892.071 44 11 -2 1 28244.5 886.282 15 -11 2 -1 29415.0 883.181 9 -11 -2 -1 28382.8 895.530 9 -11 -2 -1 27683.6 885.251 4 -11 -2 -3 8921.24 321.068 41 11 -2 3 8959.11 533.512 43 11 2 3 8911.08 348.547 44 11 -2 3 8581.94 349.037 44 -11 -2 -3 8988.24 349.444 10 -11 2 -3 8947.70 346.326 10 -11 -2 -3 9155.59 351.548 9 -11 -2 -3 9035.86 350.388 5 -11 -2 -3 8382.20 339.449 4 -11 2 -3 8546.31 337.778 4 11 -2 5 11545.9 642.954 43 11 -2 5 11531.9 453.770 44 11 2 5 12076.3 454.927 44 11 -2 5 12902.6 448.099 15 -11 -2 -5 12055.7 453.820 10 -11 2 -5 12248.0 452.660 10 -11 -2 -5 12565.3 456.711 5 -11 -2 -5 12146.0 449.446 4 -11 2 -5 12570.0 444.611 4 11 -2 7 91320.2 3031.65 43 11 -2 7 94785.3 2783.82 44 11 2 7 96417.2 2781.15 44 11 -2 7 86736.6 3121.87 45 11 2 7 91308.2 3124.87 45 11 -2 7 102023. 2759.58 15 -11 2 -7 94440.1 2769.32 10 -11 -2 -7 94738.9 2774.73 10 -11 2 -7 93941.4 2753.12 4 11 -2 9 22098.1 973.367 43 11 -2 9 24774.7 772.982 15 11 -2 9 22935.8 802.073 44 11 2 9 24551.4 806.721 44 11 -2 9 20702.1 1076.77 45 11 2 9 21292.5 1072.52 45 -11 -2 -9 25190.8 799.843 10 -11 2 -9 22587.4 784.319 10 -11 2 -9 24343.2 776.888 4 -11 -2 -11 2067.19 150.861 10 -11 2 -11 2396.47 157.608 10 11 -2 11 2000.93 287.884 45 11 -2 11 2232.69 164.333 44 11 2 11 2255.26 161.465 44 11 2 11 1976.70 285.725 45 -11 -2 -11 2383.45 150.643 16 11 -2 11 2129.12 136.950 15 -11 2 -13 117.535 49.2520 10 11 -2 13 161.015 54.7627 44 11 2 13 133.463 54.1514 44 -11 -2 -13 120.379 50.2300 16 11 -2 13 65.7485 46.2661 15 11 -2 15 48.5477 47.6817 44 11 2 15 19.9210 45.0947 44 -11 -2 -15 53.4229 41.7972 10 -11 2 -15 52.7804 43.1714 10 -11 -2 -15 46.2315 34.3768 22 -11 -2 -15 60.5024 44.5888 16 11 -2 15 17.8234 35.8105 15 -11 2 -17 1005.38 89.0134 7 -11 2 -17 908.902 86.3330 10 -11 -2 -17 847.579 84.2919 10 11 -2 17 900.970 92.5156 44 11 2 17 656.267 79.7406 44 -11 -2 -17 958.944 85.2220 16 11 -2 17 971.467 73.6915 15 11 -2 19 6856.90 274.092 44 11 2 19 6846.43 270.199 44 -11 -2 -19 7026.19 267.424 16 -11 2 -19 7569.85 272.838 7 -11 2 -19 7399.14 272.165 10 -11 -2 -19 7580.41 278.903 19 -11 -2 -21 6728.17 240.229 16 -11 2 -21 6481.54 237.125 7 -11 -2 -21 7063.59 242.655 42 -11 3 32 1012.93 61.7199 2 11 -3 -30 422.683 55.2818 6 -11 3 30 344.390 49.7721 2 -11 -3 30 295.130 36.5574 34 -11 3 28 1032.41 78.4438 8 -11 -3 28 1035.42 86.6486 8 11 -3 -28 988.268 89.8636 6 -11 -3 26 400.187 65.4981 8 -11 3 26 224.807 48.4345 8 11 -3 -26 264.071 67.2587 6 -11 -3 24 332.395 70.8735 8 11 -3 -24 419.892 82.2090 6 -11 -3 24 332.258 54.6895 2 -11 -3 24 429.063 63.2316 3 11 -3 -22 1551.09 121.591 47 11 3 -22 1401.04 114.855 47 -11 -3 22 1262.81 114.401 3 -11 -3 22 1382.85 111.945 2 11 -3 -22 1201.08 120.176 6 -11 -3 22 1416.38 128.206 8 11 -3 -20 182.291 134.468 46 11 3 -20 334.597 141.263 46 11 -3 -20 513.323 72.1102 47 11 3 -20 448.704 66.6810 47 11 -3 -20 383.235 82.1342 6 -11 -3 20 341.920 67.9372 2 -11 -3 20 410.327 70.0183 3 11 3 -20 389.504 127.653 1 -11 -3 20 515.742 81.6790 8 -11 3 20 297.894 63.6260 8 -11 3 20 242.775 129.915 13 -11 -3 20 106.602 121.820 13 11 -3 -18 1109.02 206.117 46 11 3 -18 696.936 171.215 46 11 -3 -18 983.923 99.7381 47 11 3 -18 1078.56 99.7096 47 -11 3 18 900.102 181.016 13 -11 -3 18 1333.04 221.860 13 11 3 -18 957.903 175.327 1 -11 -3 18 1112.69 109.114 2 11 -3 -18 1061.56 108.153 6 -11 -3 18 838.780 94.7904 3 -11 -3 18 1076.31 106.703 8 -11 3 18 958.069 97.8325 8 11 -3 -16 69.5222 86.1809 46 11 3 -16 45.8364 65.1012 46 11 3 -16 51.8851 41.9926 47 11 -3 -16 29.8069 32.4649 35 -11 3 16 71.7857 67.9700 13 -11 -3 16-24.0378 68.2802 13 11 -3 -16 81.3621 50.9634 6 11 3 -16 77.5032 77.8313 1 -11 -3 16 47.7628 46.9171 2 -11 -3 16 65.5192 41.6294 3 -11 -3 16 68.7431 43.6756 8 11 -3 -14 21.3210 60.5530 46 11 3 -14 21.0547 78.2910 46 11 -3 -14 4.65324 31.1967 35 -11 3 14 44.5825 79.3603 13 -11 -3 14 44.9600 72.3922 13 11 3 -14 51.9249 64.3608 1 11 -3 -14-12.6446 39.5743 6 -11 -3 14 25.8201 43.8249 2 -11 -3 14 30.6046 37.7464 3 -11 -3 14 32.0500 43.5192 8 11 -3 -12 1738.76 218.933 46 11 3 -12 1654.13 212.713 46 11 -3 -12 1668.53 107.898 35 -11 -3 12 1837.39 230.060 13 -11 -3 12 1602.06 119.912 3 -11 -3 12 1692.40 125.446 2 11 3 -12 1573.25 188.583 1 11 -3 -12 1855.59 128.612 6 -11 -3 12 1713.03 126.333 8 11 -3 -10 17647.6 782.100 46 11 3 -10 17925.4 778.821 46 11 -3 -10 16552.8 549.388 35 -11 -3 10 16596.4 573.448 3 11 3 -10 17991.3 699.625 1 -11 -3 10 17060.1 580.440 8 11 -3 -8 7506.40 443.499 46 11 3 -8 7463.22 442.753 46 11 3 -8 6039.23 359.007 43 11 -3 -8 6771.36 284.086 40 11 -3 -8 6629.04 259.859 35 -11 -3 8 7036.55 282.691 3 -11 -3 8 6694.32 281.892 8 11 -3 -6 7201.86 438.936 46 11 3 -6 7622.80 441.600 46 11 3 -6 6940.22 393.718 43 11 -3 -6 7312.93 289.001 40 11 -3 -6 6634.77 258.285 27 11 -3 -6 6545.54 262.969 15 -11 -3 6 6921.04 281.843 9 11 -3 -4 5722.68 238.439 15 -11 -3 4 5795.24 241.051 41 11 -3 -4 5838.09 250.219 40 -11 -3 4 5534.34 244.487 9 11 -3 -2 3392.97 173.250 15 -11 -3 2 3177.52 171.005 9 -11 -3 2 3234.52 166.592 41 11 -3 -2 3508.95 176.536 40 11 -3 0 112.027 45.7981 15 -11 -3 0 30.3928 30.2861 4 -11 -3 0 59.8563 36.9515 9 11 -3 0 15.8810 34.1045 44 11 3 0 15.3939 38.5657 44 -11 -3 0-4.67481 33.6728 41 11 -3 2 692.359 79.1597 44 11 3 2 865.713 84.9231 44 -11 -3 -2 775.304 77.6450 41 11 -3 2 758.288 85.8895 15 -11 -3 -2 739.627 78.5860 10 -11 3 -2 801.676 82.4956 10 -11 -3 -2 829.385 82.3307 9 -11 -3 -2 880.309 89.0136 5 -11 3 -2 829.877 80.4346 4 -11 -3 -2 814.528 79.7891 19 -11 -3 -4 735.538 84.9413 5 -11 3 -4 644.308 73.4324 4 11 -3 4 639.413 81.1073 44 11 3 4 663.212 83.3899 44 -11 -3 -4 695.276 80.1730 10 -11 3 -4 767.992 84.9486 10 -11 -3 -4 719.650 80.8454 19 -11 -3 -6 131.357 56.2197 5 -11 3 -6 187.534 48.4248 4 11 -3 6 218.009 51.3312 44 11 3 6 234.637 50.7732 44 -11 -3 -6 130.897 43.1449 16 11 -3 6 201.260 60.9946 15 -11 -3 -6 233.218 49.1851 10 -11 3 -6 259.623 50.3881 10 -11 -3 -6 182.664 57.5750 19 -11 -3 -8 35027.2 1084.43 5 -11 3 -8 33951.0 1050.56 4 -11 -3 -8 33423.8 1057.39 16 11 -3 8 36152.3 1077.95 15 11 -3 8 32753.6 1072.01 44 11 3 8 33682.6 1075.25 44 -11 -3 -8 33347.9 1060.56 10 -11 3 -8 34357.3 1068.60 10 -11 -3 -8 34560.9 1083.22 19 -11 -3 -10 671.173 82.0537 16 11 -3 10 653.351 82.7963 15 11 -3 10 496.988 78.6472 44 11 3 10 693.565 91.4132 44 -11 -3 -10 793.032 96.9502 19 -11 -3 -10 621.244 80.3068 22 -11 -3 -10 613.556 75.2427 10 -11 3 -10 641.940 79.0829 10 -11 -3 -12 1915.93 128.563 10 -11 3 -12 2166.75 137.778 10 -11 -3 -12 1855.23 133.174 16 11 -3 12 1947.86 131.003 15 11 -3 12 1953.48 139.384 44 11 3 12 1912.32 136.364 44 11 -3 12 2025.73 115.789 29 -11 -3 -12 2146.58 148.869 19 -11 -3 -12 2148.70 132.984 22 11 -3 14 2603.29 153.674 44 11 3 14 2369.84 146.791 44 -11 -3 -14 2666.41 153.639 16 11 -3 14 2547.00 142.022 15 -11 -3 -14 2466.78 139.554 10 -11 3 -14 2677.86 148.175 10 -11 -3 -14 2681.19 160.583 19 -11 -3 -14 2590.19 139.783 22 11 -3 16 1125.47 91.9032 44 11 3 16 1133.18 88.7765 44 11 -3 16 1281.07 83.6702 38 -11 -3 -16 1326.23 102.898 19 -11 -3 -16 1314.71 85.3861 22 -11 3 -16 1300.03 90.0168 10 -11 -3 -16 1320.51 97.9153 16 -11 -3 -18 341.457 50.8163 16 -11 -3 -20 4194.95 163.671 19 -11 -3 -20 4447.67 166.589 42 11 -3 20 3773.44 144.322 39 -11 3 -20 3885.46 158.021 7 -11 4 29 7436.63 251.783 2 -11 -4 29 6741.43 232.072 34 11 -4 -27 14.5425 31.7098 40 -11 -4 27 30.2688 31.0610 34 -11 -4 25-4.51282 37.5257 34 11 -4 -25 83.4261 54.2780 6 -11 -4 23 10107.2 381.705 34 11 -4 -23 10152.5 365.189 35 11 -4 -23 10608.1 413.727 6 11 -4 -21 304.486 54.9792 35 -11 -4 21 306.661 60.3581 34 11 -4 -21 394.498 79.9780 6 -11 -4 21 302.156 57.5519 8 -11 -4 19 2093.11 140.132 34 11 -4 -19 2281.66 141.875 35 11 -4 -19 2145.22 160.421 6 -11 -4 19 2162.97 144.959 8 -11 -4 17 2595.42 156.381 34 11 -4 -17 2519.63 152.990 35 11 4 -17 2374.85 255.107 1 11 -4 -17 2498.27 173.826 6 -11 -4 17 2623.63 160.419 8 -11 -4 15 32380.5 999.828 34 11 -4 -15 32568.3 1000.71 35 -11 -4 15 31798.6 1007.45 8 11 4 -15 30976.9 1205.07 1 -11 -4 13 39081.7 1146.38 34 11 -4 -13 38932.2 1150.72 35 -11 -4 13 36217.1 1148.83 8 11 -4 -13 35669.1 1167.61 40 11 -4 -11 481.677 66.8033 35 -11 -4 11 300.246 55.2392 34 -11 -4 9 48676.9 1407.73 34 11 -4 -9 47731.6 1414.85 35 -11 -4 9 45895.8 1410.77 9 11 -4 -7 46854.0 1339.44 40 11 -4 -7 44587.5 1306.96 27 -11 -4 7 43518.6 1297.45 22 -11 -4 5 23330.7 753.748 41 11 -4 -5 24244.3 767.857 40 11 -4 -5 23907.9 737.928 27 -11 -4 5 22427.0 737.075 9 -11 -4 5 23139.0 706.121 23 -11 -4 5 23142.2 746.305 22 -11 -4 3 31974.6 985.076 41 11 -4 -3 33725.5 999.653 40 -11 -4 3 31462.3 989.570 22 -11 -4 3 32497.4 939.314 23 11 -4 -3 31596.9 960.596 27 11 -4 -3 29852.8 962.216 28 -11 -4 3 30085.0 965.451 9 -11 -4 1 6160.69 270.695 5 -11 -4 1 6880.94 298.464 22 -11 -4 1 6969.76 283.984 41 -11 -4 1 6364.71 241.466 36 11 -4 -1 7432.62 268.149 27 11 -4 -1 6832.53 265.191 28 -11 -4 1 6516.27 270.418 9 -11 -4 -1 1938.04 145.175 22 -11 -4 -1 1957.84 125.495 19 -11 -4 -1 2160.25 136.600 41 -11 -4 -1 2176.08 108.518 36 11 -4 1 2203.10 150.970 15 11 -4 1 2009.23 117.081 28 11 -4 1 2435.64 126.688 27 -11 -4 -1 1933.32 130.379 5 -11 4 -1 2029.47 125.724 4 -11 -4 -3 12698.0 406.869 36 -11 -4 -3 12268.6 451.521 19 -11 -4 -3 12510.9 455.038 5 -11 -4 -5 7048.34 307.565 22 -11 -4 -5 6708.72 291.438 19 11 -4 5 6419.51 257.548 30 -11 -4 -5 6496.67 282.539 5 11 -4 5 6250.46 297.683 15 11 -4 7 63705.4 1895.03 15 11 -4 7 63071.1 1865.52 29 -11 -4 -7 60389.6 1887.38 19 -11 -4 -7 66695.3 1894.36 22 11 -4 9 41024.1 1250.92 15 11 -4 9 40314.6 1222.52 29 11 -4 9 40282.9 1215.70 37 -11 -4 -9 39594.0 1260.92 19 -11 -4 -9 41782.3 1247.43 22 11 -4 11 1987.98 118.182 29 11 -4 11 1978.54 112.362 37 -11 -4 -11 2161.66 134.153 22 -11 -4 -11 2044.53 146.303 19 11 -4 13 37.1414 26.5923 29 -11 -4 -13 61.8892 39.7100 22 -11 -4 -13-17.4875 50.4533 19 -11 -4 -15 1339.40 86.8904 22 -11 -4 -15 1316.96 102.355 19 11 -4 15 1326.15 86.8422 38 -11 -4 -17 574.106 44.1943 22 -11 -4 -17 666.669 65.5231 19 11 -4 17 687.447 49.5263 38 -11 4 -19 4342.77 161.253 7 11 -4 19 4204.93 152.313 39 11 -5 -28 9963.62 313.634 25 -11 -5 26 5782.46 204.665 34 -11 5 26 5399.24 202.668 2 -11 -5 24 21131.4 664.854 34 11 -5 -24 21119.8 649.633 35 -11 5 24 21807.3 663.456 2 -11 -5 22 4454.48 206.786 34 11 -5 -22 4936.97 204.335 35 11 -5 -22 4743.71 214.177 40 -11 -5 20 2889.07 158.135 34 11 -5 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259.472 40 12 -5 -11 5405.02 228.921 29 12 -5 -11 5542.21 245.093 27 -12 -5 9 27841.9 890.442 41 12 -5 -9 27441.3 873.688 27 12 -5 -9 28400.1 880.827 29 -12 -5 7 2297.54 146.786 41 12 -5 -7 2194.93 133.448 27 12 -5 -7 2382.78 152.936 29 12 -5 -7 1982.59 132.561 28 -12 -5 7 2268.94 130.360 22 -12 -5 7 2274.11 113.349 23 -12 -5 5 1932.45 108.602 36 -12 -5 5 2108.16 138.666 41 12 -5 -5 2097.21 124.295 27 12 -5 -5 1845.80 141.657 29 12 -5 -5 2019.26 127.774 28 -12 -5 5 1945.74 129.978 22 -12 -5 5 2236.21 111.559 23 -12 -5 3 5553.56 221.084 36 -12 -5 3 6270.88 266.029 41 12 -5 -3 6337.17 244.979 27 12 -5 -3 5664.64 277.152 29 12 -5 -3 5988.61 247.626 28 -12 -5 3 5609.07 262.175 22 -12 -5 1 21597.9 670.037 36 -12 -5 1 23032.8 722.870 41 -12 -5 1 21728.2 737.602 22 12 -5 -1 21885.6 713.477 30 12 -5 -1 21058.8 690.464 28 12 -5 -1 22620.2 692.821 27 -12 -5 -1 7969.47 275.551 36 12 -5 1 7858.34 308.431 30 12 -5 1 8208.72 341.576 29 -12 -5 -1 7460.58 337.111 22 12 -5 3 576.095 81.5373 29 12 -5 3 582.565 67.6548 30 -12 -5 -3 493.876 83.9753 22 12 -5 3 624.932 78.2354 37 12 -5 5 6471.84 267.750 29 12 -5 5 5847.77 234.043 30 12 -5 5 6219.00 260.209 37 12 -5 7 1327.64 100.698 29 12 -5 7 1412.53 100.702 37 12 -5 9 1158.13 84.5747 29 -12 -5 -9 1142.72 95.3153 22 12 -5 9 1195.34 94.8733 38 12 -5 9 1014.43 76.0083 37 12 -5 11 650.948 54.7313 29 -12 -5 -11 717.176 68.3085 22 12 -5 11 585.612 49.7251 37 12 -5 11 777.875 69.5857 38 -12 -5 -13 1114.05 72.7239 42 12 -5 13 1135.07 73.3629 38 -12 5 -15 6236.51 215.729 7 12 -5 15 5959.21 203.238 38 -12 -6 24 5555.51 198.400 41 12 -6 -24 6426.92 205.241 27 -12 -6 22 4604.60 186.652 41 12 -6 -22 5106.71 191.355 27 12 -6 -22 4840.91 178.672 25 12 -6 -22 5063.10 187.740 28 -12 -6 20 5539.42 229.789 41 12 -6 -20 6081.49 231.892 27 12 -6 -20 6199.78 235.015 28 12 -6 -20 5744.84 217.258 25 -12 -6 18 1805.89 118.896 41 12 -6 -18 2043.38 120.242 40 12 -6 -18 1991.60 118.760 27 12 -6 -18 1946.47 106.731 25 -12 -6 16 395.864 66.3966 41 12 -6 -16 411.995 64.3461 40 12 -6 -16 443.671 53.9818 25 12 -6 -16 477.544 63.7512 27 12 -6 -16 520.017 60.7904 30 -12 -6 14 5486.71 247.360 41 12 -6 -14 5706.68 251.157 40 12 -6 -14 5734.35 244.739 30 12 -6 -14 5649.31 221.715 25 12 -6 -14 5845.66 242.534 27 12 -6 -14 5860.02 253.855 28 12 -6 -12 11060.6 410.805 30 12 -6 -12 11261.4 393.901 27 12 -6 -12 10780.1 367.830 25 12 -6 -12 10757.1 402.513 28 12 -6 -10 881.741 81.2749 37 -12 -6 10 848.967 61.4208 23 12 -6 -10 978.688 99.8632 30 12 -6 -10 839.844 70.6870 29 12 -6 -10 879.023 82.3499 27 12 -6 -10 1016.41 92.5405 28 12 -6 -8 460.931 70.8144 37 12 -6 -8 534.647 65.9467 27 12 -6 -8 456.237 62.8973 29 12 -6 -8 539.147 69.7192 28 -12 -6 8 591.481 54.3153 23 12 -6 -6 62.3023 48.7102 37 12 -6 -6 119.352 58.3784 30 12 -6 -6 33.0790 46.2453 29 12 -6 -6 60.3852 38.2092 27 12 -6 -6 51.9090 41.7983 28 -12 -6 6 164.231 40.3633 22 -12 -6 6 3.29411 29.6230 36 12 -6 -4 3569.53 196.661 37 12 -6 -4 3507.36 166.885 38 12 -6 -4 3354.70 181.709 30 12 -6 -4 3402.76 162.849 27 12 -6 -4 3578.30 190.961 29 12 -6 -4 3333.70 166.727 28 -12 -6 4 3506.33 172.612 22 -12 -6 4 3404.56 149.178 36 12 -6 -2 2185.61 133.827 38 12 -6 -2 1896.32 138.845 29 12 -6 -2 2140.34 122.604 28 12 -6 -2 2275.97 122.601 27 12 -6 -2 2425.84 141.099 30 -12 -6 2 2064.45 132.941 22 -12 -6 2 2112.58 106.835 36 12 -6 0 10518.4 383.506 37 12 -6 0 9561.31 368.108 38 12 -6 0 9637.98 355.360 30 -12 -6 0 9111.50 371.281 22 -12 -6 0 9936.37 324.850 36 12 -6 2 5838.14 251.242 37 12 -6 2 5780.59 251.895 38 -12 -6 -2 5604.65 258.944 22 12 -6 2 6124.96 258.591 29 12 -6 2 5771.21 232.156 30 12 -6 4 357.124 61.5978 38 12 -6 4 225.375 47.0915 39 12 -6 4 292.976 54.3971 37 -12 -6 -4 310.443 62.4462 22 12 -6 4 338.062 43.8296 30 12 -6 4 344.568 58.7542 29 12 -6 6 1812.23 110.219 39 12 -6 6 1904.10 107.442 37 12 -6 6 1932.94 117.079 38 12 -6 6 2092.23 115.058 29 12 -6 6 1779.18 89.8526 30 12 -6 8 51.0918 31.4553 39 12 -6 8 8.00812 24.6534 37 -12 -6 -8 15.1490 33.2792 22 12 -6 8 8.86989 27.1203 29 -12 -6 -10 1215.10 75.3187 22 12 -6 10 1151.72 72.6844 39 12 -6 10 1184.23 73.6498 38 12 -6 12 2614.09 107.477 39 12 -6 12 2733.74 107.425 38 12 -7 -19 651.951 45.5247 27 12 -7 -19 570.159 43.5116 28 12 -7 -17 864.014 60.0989 27 12 -7 -17 785.833 60.2962 28 -12 -7 17 860.717 59.2876 41 -12 -7 15 1235.57 79.7610 41 12 -7 -15 1229.93 76.3197 27 12 -7 -15 1247.65 75.1938 24 -12 -7 15 1075.09 62.1366 36 -12 -7 13 74.3057 35.2250 41 12 -7 -13 6.24358 30.7151 30 12 -7 -13 22.0387 28.6794 27 12 -7 -13 58.6377 35.1885 28 12 -7 -13 31.1634 33.6598 24 -12 -7 13-15.9135 24.8896 36 12 -7 -11 2030.63 107.791 27 12 -7 -11 2223.84 117.919 28 12 -7 -11 1976.55 115.334 30 -12 -7 11 2037.89 114.091 41 -12 -7 11 1910.57 94.7248 36 12 -7 -9 2972.35 138.026 27 12 -7 -9 3264.39 149.629 28 12 -7 -9 2885.67 152.742 30 -12 -7 9 2966.39 145.679 41 -12 -7 9 2967.35 126.236 36 12 -7 -7 4227.98 179.780 28 12 -7 -7 4092.94 170.194 27 -12 -7 7 4050.73 180.006 41 12 -7 -7 3947.39 174.431 37 -12 -7 7 4110.79 157.484 36 12 -7 -5 8469.91 308.172 30 12 -7 -5 7949.17 300.000 37 -12 -7 5 8060.00 269.174 36 12 -7 -3 1293.91 95.3012 37 12 -7 -3 1284.95 92.2496 29 12 -7 -3 1394.82 94.1780 30 12 -7 -3 1204.08 84.0575 24 -12 -7 3 1303.37 70.8331 36 12 -7 -1 65.5198 31.0869 24 12 -7 -1 88.4097 35.8271 30 12 -7 -1 85.2801 38.5583 29 12 -7 1 9.02022 26.8094 38 12 -7 1 45.8417 36.3059 37 12 -7 1-1.89504 18.9736 24 12 -7 1-11.4158 28.7380 30 12 -7 3 5380.30 192.222 30 12 -7 3 5719.10 207.969 37 12 -7 3 5260.09 202.266 38 12 -7 5 734.952 43.4840 30 12 -7 5 1114.60 65.2903 38 12 -7 7 547.936 38.3388 32 12 -7 7 534.874 37.6032 31 12 -8 -10-5.16300 16.7289 24 12 -8 -8 5726.24 199.773 30 12 -8 -8 6384.15 204.558 24 12 -8 -6 564.569 41.8430 24 12 -8 -4 4139.13 149.590 30 12 -8 -2 93.9422 20.4722 30 -13 0 33-2.20469 17.0654 3 -13 0 33-2.48329 23.0847 8 13 0 -31 18.9009 23.1882 6 -13 0 31 6.03266 26.3049 2 -13 0 31-4.08781 33.7049 8 13 0 -29-27.7177 32.9247 6 -13 0 29 4.40660 37.5453 2 -13 0 29 5.57819 45.9933 8 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18.8835 44.3087 3 -13 0 9 10.4925 35.6195 2 -13 0 7 24.3018 38.0286 8 13 0 -7 38.7383 74.9641 43 -13 0 7 6.08063 37.4972 3 -13 0 7 14.9141 33.3280 2 -13 0 5 11.8669 37.1373 9 13 0 -5 39.6386 76.7050 43 -13 0 5-11.9861 36.9546 3 13 0 -3 61.7923 45.9866 44 13 0 -3 61.7230 79.6463 43 -13 0 3 64.6716 41.4195 9 13 0 -1 43.2538 61.4244 43 13 0 -1 44.5224 50.6379 44 -13 0 1 11.9014 39.3830 9 13 0 1-6.71000 48.3178 44 -13 0 -1-18.3224 38.7866 9 13 0 3 23.6337 76.1072 43 -13 0 -3 34.0443 45.6450 10 -13 0 -3-6.35982 43.7145 9 13 0 3 36.0570 56.3554 44 13 0 5 48.3703 82.0954 43 -13 0 -5 7.16547 44.8506 10 13 0 5 46.3909 56.2908 44 -13 0 -5 31.1119 40.6300 5 -13 0 -5-20.6434 48.9967 4 13 0 7-24.0497 68.3043 43 -13 0 -7 66.8819 46.5183 10 13 0 7 40.8925 57.5714 44 -13 0 -7-7.10398 51.1584 4 -13 0 -7 37.9588 45.0515 5 13 0 9 23.0096 55.2314 43 -13 0 -9-18.8571 47.7134 5 13 0 9-75.3745 73.5866 44 -13 0 -9-14.8543 56.3762 10 13 0 11-8.10078 60.8680 44 -13 0 -11 7.06204 57.2310 10 -13 0 -13 20.8478 31.3294 7 -13 0 -13 19.0265 44.1190 10 13 0 13-51.2849 54.4848 44 -13 0 -15 5.32622 45.7404 10 13 0 15 30.6043 43.5845 44 13 0 15 18.3577 32.0213 15 -13 0 -17 20.9569 37.1007 10 -13 0 -17 19.8995 28.2578 16 13 0 17 10.9022 26.1683 15 13 0 17-18.8789 37.9124 44 -13 0 -19 6.73182 20.9992 16 -13 0 -19 8.22383 24.0862 19 13 -1 -32 3649.57 140.823 6 -13 1 32 3511.07 142.287 2 -13 1 32 3607.82 149.545 8 -13 -1 32 3364.23 148.968 8 -13 -1 30 454.384 51.9687 2 13 -1 -30 613.820 61.4187 6 -13 1 30 592.305 62.2433 2 -13 1 30 544.180 67.1658 8 -13 -1 28 18387.3 596.895 2 13 -1 -28 18524.0 603.953 6 13 1 -28 16964.2 572.834 6 13 -1 -26 39975.0 1198.98 6 -13 -1 26 38571.9 1195.97 2 13 1 -26 37407.3 1165.36 6 13 -1 -26 38230.6 1217.58 47 13 1 -26 39395.2 1217.49 47 -13 1 26 41712.4 1232.03 8 -13 1 24 9921.82 392.624 2 -13 -1 24 9514.76 386.386 2 13 -1 -24 9190.35 375.082 6 13 -1 -24 9800.92 403.357 47 13 1 -24 9633.58 396.345 47 -13 1 22 4021.17 220.836 2 -13 -1 22 3960.40 222.401 2 13 -1 -22 4121.38 212.637 6 13 -1 -22 3931.93 419.733 46 13 1 -22 3664.02 394.689 46 13 -1 -22 3964.65 227.700 47 13 1 -22 4494.72 236.078 47 -13 1 22 3614.57 401.438 13 -13 -1 22 3455.82 390.863 13 -13 1 20 53723.4 1589.17 2 13 -1 -20 50772.2 1562.54 6 -13 -1 20 51054.4 1589.17 2 -13 1 20 52620.4 1601.71 8 13 -1 -20 52307.5 1986.53 46 13 1 -20 52978.1 1972.69 46 13 1 -20 52796.3 1586.15 47 -13 1 20 49768.1 1968.51 13 -13 -1 20 49879.4 1977.63 13 -13 1 18 36634.7 1128.02 2 13 -1 -18 34733.4 1100.76 6 -13 1 18 36506.6 1139.26 8 13 -1 -18 35276.0 1472.18 46 13 1 -18 34730.5 1448.20 46 -13 1 18 35232.0 1489.35 13 -13 -1 18 35081.7 1487.83 13 -13 1 16 2151.24 146.669 2 13 -1 -16 1897.17 126.921 6 -13 1 16 2035.36 147.027 8 13 1 -16 1931.12 259.703 46 13 -1 -16 1687.91 253.842 46 -13 1 16 1326.97 231.946 13 -13 -1 16 1409.27 245.745 13 13 -1 -14 449.695 60.6080 6 -13 -1 14 515.805 85.3581 3 -13 -1 14 604.176 83.2493 2 -13 1 14 462.305 73.7966 2 -13 1 14 434.700 73.3205 8 13 -1 -14 324.549 131.933 46 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8549.46 337.614 4 -13 1 4 8530.53 340.440 3 13 1 -2 13416.6 691.909 43 -13 1 2 13958.7 481.304 9 13 -1 -2 13305.7 491.603 44 13 1 -2 13618.3 488.115 44 -13 -1 2 12799.7 473.494 4 13 1 0 1489.29 215.717 43 13 -1 0 1212.89 200.963 43 -13 1 0 1538.79 115.811 9 13 -1 0 1357.83 119.898 44 13 1 0 1601.92 125.884 44 -13 -1 0 1579.37 118.384 4 -13 1 0 1655.37 123.330 4 13 1 2 1892.31 247.739 43 13 -1 2 1823.40 248.820 43 -13 1 -2 1838.13 128.983 9 -13 -1 -2 1788.23 132.356 10 13 1 2 1869.13 139.965 44 13 -1 2 1877.45 141.073 44 -13 -1 -2 1596.25 126.792 4 -13 1 -2 1836.16 131.612 4 13 -1 4 13698.9 739.717 43 -13 -1 -4 14180.5 520.731 10 -13 1 -4 13665.2 514.129 10 13 -1 4 13728.0 527.205 44 13 1 4 14223.4 527.208 44 -13 1 -4 13832.2 495.557 5 -13 -1 -4 14250.5 514.213 5 -13 -1 -4 14092.9 515.746 4 -13 1 -4 14810.7 516.331 4 13 -1 6 1045.18 189.151 43 -13 -1 -6 1078.89 107.496 10 -13 1 -6 942.890 101.981 10 13 -1 6 995.491 111.188 44 13 1 6 899.146 107.420 44 -13 1 -6 907.971 89.4005 5 -13 -1 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74.5700 22 -18 3 1 637.374 64.4508 10 -18 -3 1 809.074 76.0474 5 -18 3 1 808.226 74.4214 4 -18 -3 -1 3727.02 170.064 22 -18 -3 -1 4019.02 176.108 5 -18 3 -1 3981.18 168.869 4 18 -3 3 6223.73 218.125 29 -18 3 -3 5335.81 204.495 10 18 -3 5 36.4528 21.9714 29 -18 3 -5 21.2088 14.3456 10 -18 -3 -5 52.1515 28.8789 22 -18 -3 -7 7424.59 244.086 22 18 -4 -22 13.8994 19.7371 40 18 -4 -22-3.42626 15.2751 28 -18 -4 20 10436.9 344.937 41 18 -4 -20 10871.4 349.680 28 -18 -4 18 1989.19 95.6319 41 18 -4 -18 2162.97 111.924 40 18 -4 -18 1842.92 92.7354 28 -18 -4 16 3915.26 155.381 41 18 -4 -16 3693.17 149.304 28 -18 -4 14 4202.02 166.753 41 18 -4 -14 4071.02 156.934 28 -18 -4 12 2319.79 110.822 41 -18 4 12 2102.60 121.373 4 -18 4 10-7.90275 34.4788 4 -18 -4 10 70.4953 30.2660 41 18 -4 -10 71.0202 32.4918 29 -18 4 8 2904.70 144.978 4 18 -4 -8 3204.94 149.408 29 -18 4 6 7311.18 267.989 4 18 -4 -6 7224.03 274.947 29 -18 4 4 35.4857 28.1466 4 -18 -4 4 16.0127 27.9423 22 18 -4 -4 32.1699 27.4659 30 18 -4 -4 58.1316 34.8164 29 -18 4 2 3149.67 136.920 4 -18 -4 2 3564.05 149.685 22 18 -4 -2 3154.99 123.603 30 -18 -4 0 583.946 58.1574 22 18 -4 0 774.522 58.8033 37 18 -4 0 639.548 58.5997 29 -18 -4 -2 610.444 52.9952 22 18 -4 2 579.570 50.1322 29 18 -4 2 653.825 48.0809 37 18 -4 4 11.8099 17.2786 29 18 -5 -17 203.499 29.0032 30 -18 -5 17 201.412 25.8765 41 -18 -5 15 6375.62 214.615 41 18 -5 -13 7752.26 248.068 30 -18 5 13 6323.47 225.042 4 18 -5 -11 1452.90 81.7406 30 18 -5 -11 1327.44 72.5626 37 18 -5 -9-2.73770 25.2795 37 18 -5 -9-5.36542 29.7874 30 18 -5 -7 1917.49 100.421 37 18 -5 -7 1905.34 94.1150 29 18 -5 -7 2163.90 97.1937 30 18 -5 -5 6443.09 227.004 29 18 -5 -5 6504.25 216.227 30 18 -5 -3 64.7658 27.0888 37 18 -5 -3 89.9051 27.5524 29 18 -5 -1 1467.22 72.2754 37 18 -5 1 4753.16 160.225 29 -19 0 27-15.4708 17.8619 9 -19 0 25-12.3362 28.8617 9 -19 0 23 4.05541 34.2764 3 19 0 -23-4.17060 31.6554 47 -19 0 23 7.97100 35.2778 9 -19 0 21 4.76752 39.3119 3 19 0 -21 42.7914 42.3972 47 -19 0 21 14.0280 40.1577 9 -19 0 19-5.26737 42.6879 3 -19 0 19-12.0937 32.3827 4 -19 0 19-10.3004 45.2515 9 -19 0 17-11.1603 43.6106 3 -19 0 17 37.0111 36.8339 4 -19 0 17 43.6248 46.0938 9 -19 0 15 10.0692 35.4376 4 -19 0 15-5.64274 44.9196 9 -19 0 13-10.6104 41.4588 4 -19 0 13-11.4673 48.8508 9 -19 0 11-21.8884 42.7624 4 -19 0 11 17.2596 49.4047 9 -19 0 9-5.52662 45.1795 4 -19 0 9-11.4047 43.2821 9 -19 0 7 16.5684 43.1584 4 -19 0 7-5.61007 44.6597 9 -19 0 5-5.19003 40.5587 5 -19 0 5 21.7762 42.9433 4 -19 0 5-5.90458 49.5024 10 -19 0 5 38.2834 43.9320 9 -19 0 3-4.95862 39.1131 5 -19 0 3-21.1306 43.9229 4 -19 0 3 34.3049 44.2559 10 19 0 -1-3.49691 28.3392 15 -19 0 1-18.3995 38.5635 5 -19 0 1 25.0669 40.9836 4 -19 0 1-5.40519 44.5657 10 19 0 1 6.79247 27.2807 15 -19 0 -1 8.20357 34.1046 5 -19 0 -1-19.7914 42.8190 10 19 0 3 3.08239 27.0826 15 -19 0 -3-12.8544 36.7947 10 19 0 5 10.4577 24.3081 15 -19 0 -5 27.6052 27.7218 10 19 0 7 26.0906 20.6758 15 -19 1 26 156.530 25.0151 9 -19 1 26 162.184 29.0998 3 -19 1 24 14639.8 427.247 9 -19 1 24 15500.3 438.686 3 19 -1 -22 5386.53 207.041 40 -19 1 22 6028.46 231.943 9 19 -1 -22 5825.24 236.190 47 19 1 -22 6111.29 236.749 47 -19 1 22 5935.46 235.706 3 19 -1 -20 4106.37 172.207 40 -19 1 20 4318.37 195.485 9 19 -1 -20 4272.62 198.991 47 19 1 -20 4609.66 200.370 47 -19 1 20 4651.90 204.129 3 -19 1 18 5338.62 226.519 3 19 -1 -18 4579.39 188.188 40 -19 1 18 4776.50 215.023 9 -19 -1 18 4876.77 225.167 9 -19 1 16 25.2611 41.6645 9 -19 -1 16 39.0267 45.9760 9 -19 1 14 2437.24 145.304 9 -19 -1 14 2262.90 150.632 9 -19 -1 14 2606.15 138.000 4 -19 1 12 1574.32 113.797 9 -19 -1 12 1774.55 126.541 9 -19 -1 12 1500.47 105.723 4 -19 1 12 1352.02 110.916 4 -19 1 10 12891.9 459.978 9 -19 -1 10 13388.1 474.921 9 -19 -1 10 12632.8 452.762 4 -19 1 10 13406.6 470.770 4 -19 1 8 56.4451 37.3637 9 -19 -1 8 5.72565 45.5847 9 -19 -1 8 10.0941 39.0725 4 -19 -1 6 1862.74 129.511 10 -19 1 6 1975.75 133.251 10 -19 1 6 1840.13 121.068 9 -19 -1 6 1728.27 127.234 9 -19 -1 6 1676.74 117.000 4 -19 -1 4 13910.2 497.436 10 -19 1 4 14157.5 498.243 10 -19 1 4 14131.1 478.785 5 -19 -1 4 14422.0 494.453 5 -19 -1 4 14140.3 487.280 4 -19 -1 2 8311.22 329.959 10 -19 1 2 8298.91 330.020 10 -19 1 2 8346.94 310.232 5 -19 -1 2 9344.59 334.377 5 -19 -1 2 8344.81 321.428 4 -19 1 2 8823.46 332.101 4 19 -1 -2 8166.88 298.950 15 -19 -1 0 2100.15 131.112 10 -19 1 0 2317.56 135.746 10 -19 1 0 2138.33 115.204 5 -19 -1 0 2366.03 132.308 5 -19 1 0 2331.02 134.773 4 19 -1 0 1936.64 111.268 15 19 1 0 2155.51 110.625 15 -19 -1 -2 125.973 41.3324 10 -19 1 -2 121.097 40.3598 10 -19 -1 -2 160.358 43.6046 5 19 -1 2 121.637 34.3959 15 19 1 2 122.545 32.5952 15 19 -1 4 25.8088 25.9499 15 19 1 4 26.2248 24.8748 15 -19 -1 -4 42.6410 26.7124 10 -19 1 -4 25.0584 29.5265 10 19 -1 6 8954.19 295.963 15 19 1 6 8621.57 291.155 15 -19 -1 -6 9659.69 299.079 22 -19 -1 -6 9104.72 303.046 10 -19 1 -6 9263.69 305.003 10 19 1 8 421.252 31.4567 15 -19 -2 25 3751.78 141.373 9 19 -2 -23 2177.96 100.745 40 -19 -2 23 2097.26 108.093 9 19 -2 -21 1636.72 90.0573 40 -19 2 21 1385.23 83.1948 9 -19 -2 21 1409.63 94.6757 9 19 -2 -19 8818.80 311.044 40 -19 2 19 9175.18 314.107 9 -19 -2 19 9252.59 333.705 9 19 -2 -19 9095.76 328.041 47 19 2 -19 8534.55 320.011 47 -19 2 17 230.552 44.8364 9 -19 -2 17 233.608 54.3786 9 19 -2 -17 203.770 40.5453 40 -19 2 15 377.798 53.5775 9 -19 -2 15 425.082 63.4906 9 19 -2 -15 449.093 52.8951 40 -19 2 13 2167.54 124.136 9 -19 -2 13 2217.00 138.498 9 -19 2 11 8209.97 319.963 4 -19 2 11 7963.69 299.441 9 -19 -2 11 7995.50 318.932 9 -19 2 9 2198.30 139.457 4 -19 2 9 2315.88 125.524 9 -19 -2 9 2333.99 140.657 9 -19 2 7 3009.56 147.248 5 -19 -2 7 3205.05 169.197 5 -19 2 7 3208.85 170.018 4 -19 -2 7 3102.58 164.376 10 -19 2 7 3370.71 170.198 10 -19 -2 7 3164.62 169.449 9 -19 2 5 20904.8 673.067 5 -19 -2 5 21860.0 705.903 5 -19 2 5 22456.1 708.988 4 -19 -2 5 22411.7 705.069 10 -19 2 5 22728.3 707.295 10 -19 2 3 6314.95 237.145 5 -19 2 3 6820.18 269.031 4 -19 -2 3 6632.44 265.230 10 -19 2 3 6778.24 267.728 10 19 -2 -1 235.224 40.1410 15 -19 2 1 323.009 53.6658 4 -19 -2 1 215.310 47.1837 10 -19 2 1 272.101 51.1000 10 19 -2 1 24.9499 26.7814 15 19 2 1 15.6504 22.7463 15 -19 2 -1-7.47612 31.5941 4 -19 -2 -1-21.8267 33.3629 10 -19 2 -1-7.41445 28.6956 10 -19 -2 -3 11.4969 23.5053 10 -19 2 -3 18.0811 26.0873 10 19 2 3 39.5998 23.0617 15 19 -2 5 2241.22 94.9085 29 19 2 5 2477.30 102.432 15 -19 2 -5 2474.32 106.627 10 -19 -2 -7 3847.84 133.997 22 19 -3 -22 584.426 46.8664 40 19 -3 -20 230.964 37.9194 40 19 -3 -20 183.755 26.7709 28 -19 -3 18 1326.72 83.7545 9 19 -3 -18 1565.98 87.1303 40 -19 -3 16 15.0408 27.6741 9 -19 -3 14 8.05066 32.6235 9 -19 3 14 21.3716 35.5411 4 -19 3 12 77.7174 31.8587 10 -19 -3 12 108.382 41.3140 9 -19 3 12 60.9534 39.7183 4 -19 3 10 361.385 49.2386 10 -19 -3 10 404.091 56.8274 9 -19 -3 10 295.587 50.4209 5 -19 3 10 468.983 60.9306 4 -19 3 8 1785.89 105.109 10 -19 -3 8 1894.01 112.631 5 -19 3 8 1756.93 111.406 4 -19 3 6 5939.89 237.062 10 -19 -3 6 6520.68 250.340 5 -19 3 6 6508.75 249.980 4 -19 -3 4 503.590 53.1262 22 19 -3 -4 422.645 41.1021 30 -19 -3 4 459.557 57.7881 5 -19 3 4 586.975 61.0840 4 -19 3 4 385.045 48.7901 10 -19 -3 2 1846.15 104.692 5 -19 3 2 1864.61 101.028 4 -19 3 2 1509.66 88.2939 10 -19 -3 2 1701.21 97.0446 22 -19 3 0 1015.77 63.4875 10 -19 -3 0 1302.37 78.7564 22 -19 -3 -2 1917.24 93.5199 22 19 -3 2 1701.94 79.7747 37 19 -3 2 1910.51 90.1024 29 19 -3 4 436.516 32.5177 29 -19 4 19 13548.3 420.831 4 -19 4 17 76.3092 28.7401 4 -19 4 15 330.266 43.4583 4 -19 4 13 966.152 69.9611 4 -19 4 11 4476.63 179.302 4 -19 4 9 5678.41 212.437 4 19 -4 -9 5690.53 206.372 29 -19 4 7 19.0835 23.7777 4 19 -4 -7-4.78152 23.3839 30 19 -4 -7 49.0045 29.5203 29 -19 4 5 18695.7 561.175 4 19 -4 -5 19408.9 574.078 29 19 -4 -5 17944.0 548.464 30 -19 4 3 5163.73 194.544 4 19 -4 -3 7469.46 223.816 37 -19 -4 1 861.692 53.4695 22 19 -4 -1 826.426 54.3215 37 19 -4 1 1151.39 58.3023 29 -19 -4 -1 1089.47 57.1079 22 19 -4 1 1092.43 56.7682 38 19 -5 -12 1243.60 62.9512 30 19 -5 -10 3800.33 136.277 30 19 -5 -8 1623.65 73.1675 37 19 -5 -6 2472.00 97.9179 37 -20 0 24 49222.9 1408.98 9 -20 0 22 13087.1 426.271 9 20 0 -20 363.768 52.1047 47 -20 0 20 430.523 55.1879 9 -20 0 18 1211.46 90.1953 9 -20 0 16 1085.80 81.1563 4 -20 0 16 1007.84 86.2673 9 -20 0 14 2630.12 139.773 4 -20 0 14 2641.17 145.733 9 -20 0 12 1126.83 89.9904 4 -20 0 12 1084.52 92.2376 9 -20 0 10 53538.8 1584.71 4 -20 0 10 54297.5 1590.28 9 -20 0 8 2523.77 141.780 4 -20 0 8 2727.69 152.089 10 -20 0 8 2560.93 145.597 9 -20 0 6 684.605 68.6013 5 -20 0 6 633.787 71.5966 4 -20 0 6 830.444 81.1845 10 -20 0 4 9805.54 338.825 5 -20 0 4 8826.55 335.989 4 -20 0 4 9292.74 347.832 10 -20 0 2 1525.14 95.4648 5 -20 0 2 1528.54 99.6034 4 -20 0 2 1426.65 101.853 10 -20 0 0 5981.32 226.461 5 -20 0 0 6240.12 241.249 10 -20 0 -2 604.656 57.6766 10 20 0 4 8976.86 282.072 15 -20 1 23 1253.07 69.3187 9 -20 1 21 26.7308 24.9045 9 -20 -1 21 24.1592 31.8722 9 -20 1 21 8.04788 22.1233 4 -20 1 19 193.753 40.5937 9 -20 -1 19 148.232 40.5606 9 -20 1 19 149.844 36.9788 4 20 -1 -19 148.504 39.7104 47 20 1 -19 126.841 38.9325 47 -20 1 17 2828.99 141.306 4 -20 1 17 2744.47 139.635 9 -20 -1 17 2850.17 148.699 9 -20 1 15 1907.99 116.986 4 -20 1 15 2165.26 119.866 9 -20 -1 15 1880.57 122.083 9 -20 1 13 49.7916 40.7384 4 -20 1 13 105.924 40.7651 9 -20 -1 13 148.129 48.1889 9 -20 -1 11 7443.33 286.230 4 -20 1 11 7802.81 302.693 4 -20 1 11 7967.85 298.009 9 -20 -1 11 8479.49 312.266 9 -20 -1 9 2271.80 124.394 4 -20 1 9 2349.53 135.270 4 -20 -1 9 2190.15 134.971 10 -20 1 9 2186.39 134.562 10 -20 1 9 2464.48 131.395 9 -20 -1 9 2250.68 135.477 9 -20 1 7 1824.39 107.937 5 -20 -1 7 1919.43 120.636 5 -20 -1 7 1675.72 107.380 4 -20 -1 7 1902.22 120.533 10 -20 1 7 1944.77 122.118 10 -20 -1 7 1861.37 120.817 9 -20 1 5 1074.62 77.6723 5 -20 -1 5 1086.40 89.3403 5 -20 -1 5 1052.75 82.6001 4 -20 -1 5 1030.69 88.0355 10 -20 1 5 1058.11 88.9808 10 -20 1 3-12.7838 25.6731 5 -20 -1 3 12.0456 34.4803 5 -20 1 3-12.3702 39.0908 4 -20 -1 3-12.9699 36.2455 10 -20 1 3-12.8828 34.4952 10 -20 1 1 10.7508 22.5329 5 -20 -1 1 10.8212 29.7406 5 -20 1 1 18.6242 31.4826 4 -20 -1 1-11.6520 32.5619 10 -20 1 1-11.6203 34.5372 10 -20 -1 -1 172.583 38.1010 10 -20 1 -1 157.043 37.6275 10 -20 -1 -3 155.542 28.8820 10 -20 1 -3 164.518 30.6939 10 -20 -1 -5 276.167 26.8772 22 -20 2 22 630.767 47.2971 4 -20 -2 22 635.818 48.3177 9 -20 2 20 2343.26 115.627 4 -20 -2 20 2669.62 121.807 9 -20 2 18 4180.78 171.850 4 -20 -2 18 4375.41 176.395 9 -20 2 16 2628.34 120.805 9 -20 -2 16 2762.74 138.799 9 -20 2 14 179.711 36.7500 9 -20 -2 14 183.519 47.2213 9 -20 2 12 3744.21 172.251 4 -20 2 12 3301.82 149.733 9 -20 -2 12 3742.68 171.733 9 -20 2 10 22433.8 696.458 5 -20 -2 10 22917.3 722.105 5 -20 2 10 24081.0 727.391 4 -20 -2 10 22579.1 717.595 10 -20 2 10 22876.4 719.868 10 -20 -2 10 23936.7 727.134 9 -20 2 8 10899.2 367.829 5 -20 -2 8 11011.3 393.384 5 -20 2 8 12412.8 403.208 4 -20 -2 8 11752.2 394.502 10 -20 2 8 11342.5 392.793 10 -20 2 6 7237.48 261.394 5 -20 -2 6 8122.47 295.271 5 -20 2 6 8534.88 298.051 4 -20 -2 6 7876.79 289.691 10 -20 2 6 8136.40 292.137 10 -20 2 4 382.408 53.0127 4 -20 -2 4 280.886 45.7023 10 -20 2 4 288.991 45.9174 10 -20 -2 4 346.281 43.9788 22 -20 2 2 4199.49 173.793 4 -20 -2 2 3922.51 166.898 10 -20 2 2 4145.45 171.078 10 -20 -2 2 4229.95 166.969 22 -20 2 0 810.664 59.4156 10 -20 -2 0 881.153 60.0109 22 20 -2 2 1356.41 68.2337 29 -20 2 -2 1424.34 70.6377 10 -20 3 19 1019.91 66.0465 4 -20 3 17 1555.19 88.5863 4 -20 -3 15 144.754 31.1511 9 -20 3 15 135.417 33.2417 4 -20 3 13 42.9304 24.1424 10 -20 -3 13 124.402 30.6523 9 -20 -3 13 119.205 30.1975 5 -20 3 13 104.228 34.5162 4 -20 -3 11 8479.86 280.278 5 -20 3 11 8846.64 288.855 4 -20 -3 9 6555.92 232.251 5 -20 3 9 6931.42 238.193 4 -20 3 7-4.74951 20.2327 10 -20 -3 7 15.3670 25.5540 5 -20 3 7-6.26972 27.3372 4 -20 -3 5 9540.24 291.226 5 -20 3 5 9896.23 293.208 4 -20 -3 3 3720.60 149.226 5 -20 3 3 3729.39 146.758 4 20 -3 -1 2875.90 111.781 29 20 -3 -1 2667.67 104.388 37 20 -3 1 2520.34 95.9662 29 20 -4 -16 2821.23 108.005 30 20 -4 -14 3668.06 136.552 30 -20 4 14 3603.97 135.112 4 20 -4 -12 705.521 48.0783 30 -20 4 12 675.948 47.3631 4 20 -4 -10 2830.15 107.936 30 -20 4 10 2558.18 106.831 4 20 -4 -10 2762.22 111.170 37 20 -4 -8 959.204 59.2769 37 20 -4 -6 4414.06 154.652 29 20 -4 -4 615.750 41.0577 29 20 -4 -4 731.898 44.4386 37 -21 0 21-13.6776 22.0256 9 -21 0 19-5.71667 26.2148 9 -21 0 17-16.3040 30.7170 9 -21 0 15-3.51496 29.9472 9 -21 0 13 3.23394 26.2079 4 -21 0 13-3.64324 32.4845 9 -21 0 11 6.86008 27.0577 4 -21 0 11-12.0490 32.2635 10 -21 0 11 44.3297 32.7004 9 -21 0 9-3.48471 27.7417 5 -21 0 9 3.49212 27.8007 4 -21 0 9 44.0123 34.3597 10 -21 0 7-16.6027 28.9567 5 -21 0 7 3.43118 26.8132 4 -21 0 7 31.0162 26.9707 10 -21 0 5 15.1695 27.4407 5 -21 0 5 22.7484 26.1042 4 -21 0 5-43.6966 32.7024 10 -21 0 3-23.6809 23.2943 5 -21 0 3-3.28645 28.6625 10 -21 1 20 1084.80 61.5576 9 -21 -1 20 1307.91 73.9040 9 -21 1 18 8073.13 280.637 4 -21 1 18 8224.41 280.661 9 -21 1 16 11570.1 391.978 4 -21 1 16 12250.3 390.950 9 -21 -1 16 12528.5 403.270 9 -21 1 14 2565.46 126.592 4 -21 1 14 2743.42 126.688 9 -21 -1 14 2643.53 131.742 9 -21 1 12 3072.29 145.327 4 -21 -1 12 3022.75 147.748 10 -21 1 12 3262.82 151.627 10 -21 1 12 3210.62 142.960 9 -21 -1 12 3395.23 153.817 9 -21 1 10 10870.4 357.499 5 -21 -1 10 11224.8 370.638 5 -21 1 10 10399.0 365.301 4 -21 -1 10 10461.9 368.954 10 -21 1 10 11035.7 372.627 10 -21 1 8 213.813 37.4353 5 -21 -1 8 237.205 44.8840 5 -21 1 8 297.993 47.5488 4 -21 -1 8 272.402 44.7587 10 -21 1 8 311.802 47.1413 10 -21 1 6 5789.26 211.261 5 -21 -1 6 6118.99 227.759 5 -21 -1 6 6118.09 229.824 10 -21 1 6 5930.78 228.558 10 -21 1 4 788.461 52.9941 5 -21 -1 4 914.414 65.7308 5 -21 -1 4 897.663 67.1708 10 -21 1 4 875.019 67.8727 10 -21 -1 2 4383.87 161.341 5 -21 -1 2 3709.52 156.484 10 -21 1 2 4150.86 161.869 10 -21 -1 2 3948.95 149.890 22 -21 -1 0 5322.64 183.058 10 -21 1 0 5568.71 185.859 10 -21 2 19 1438.59 71.8420 4 -21 -2 19 1375.01 71.5369 9 -21 2 17 4620.23 168.689 4 -21 2 17 4019.36 158.722 10 -21 -2 17 4411.68 166.758 9 -21 -2 15 507.567 48.6685 5 -21 2 15 403.049 43.8040 10 -21 2 13 62.8083 17.8983 5 -21 -2 13 86.4973 30.7894 5 -21 2 13 102.479 30.3308 10 -21 -2 13 111.440 32.8014 9 -21 -2 11 3041.60 136.622 5 -21 2 11 3198.32 139.666 4 -21 2 11 2933.70 133.154 10 -21 -2 9 160.038 35.2143 5 -21 2 9 167.616 36.2845 4 -21 2 9 135.188 31.6161 10 -21 -2 7 88.3089 30.7701 5 -21 2 7 138.657 34.8093 4 -21 2 7 95.0634 29.4419 10 -21 2 5 11834.8 364.893 4 -21 2 5 10621.1 354.299 10 -21 2 3 5408.18 186.518 10 21 -2 -1 1540.54 68.9728 29 -21 3 16 856.481 51.8378 4 -21 3 14-6.50320 17.4135 4 -21 3 12 47.3434 21.9524 4 -21 3 10 572.443 45.3800 4 -21 3 8 1085.87 59.9106 4 21 -3 -8 898.821 52.0452 29 21 -3 -6 16.7088 15.2257 29 -22 0 18 1529.35 74.0003 10 -22 0 16 2124.34 99.9324 10 -22 0 16 2307.97 98.6877 9 -22 0 16 2235.86 97.2513 5 -22 0 14 229.006 35.0431 10 -22 0 14 263.440 33.7770 5 -22 0 12 6550.78 226.693 10 -22 0 12 6014.48 216.714 5 -22 0 10 1452.97 79.8324 10 -22 0 10 1472.50 75.6506 5 -22 0 8 2003.12 91.2669 5 -22 0 6 10598.3 329.650 5 -22 -1 17 384.769 35.7082 9 -22 -1 15 734.943 49.9061 10 -22 1 15 627.581 48.4129 10 -22 -1 13 3289.22 132.638 10 -22 1 13 3310.33 133.870 10 -22 1 13 3029.14 126.853 4 -22 -1 11 41.0263 21.0820 10 -22 1 11 64.1059 23.4074 10 -22 -1 11 40.4310 22.4361 5 -22 1 11 38.5643 20.6994 4 -22 -1 9 60.9369 20.4503 10 -22 1 9 40.7487 19.0944 10 -22 -1 9-13.7732 20.3312 5 -22 1 9 22.6294 19.5963 4 -22 -1 7 1300.09 70.5259 10 -22 1 7 1463.20 74.1738 10 -22 -1 7 1381.00 71.5431 5 -22 1 7 1410.06 72.2295 4 -22 -1 5 1911.26 82.9956 5 -22 2 10 1985.33 86.2645 4 0 0 0 0.00 0.00 0 TITL AS500 in I2/a REM I2/a (#15 in standard setting) CELL 1.54184 17.804573 7.602221 27.759457 90.0000 108.4869 90.0000 ZERR 1.00 0.000188 0.000058 0.000292 0.0000 0.0011 0.0000 LATT 2 SYMM -x+1/2, y,-z SFAC C H B F S Cl UNIT 136.00 152.00 8.00 40.00 8.00 8.00 TREF HKLF 4 END ; _shelx_hkl_checksum 69936 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.395 _oxdiff_exptl_absorpt_empirical_full_min 0.603