The Effect of Thermal Processing Parameters on the Microstructure of Extruded and Sintered TiO2 Ceramics
IOP Conference Series: Materials Science and Engineering 2013
Agnese Pūra, Jānis Ločs, Līga Bērziņa-Cimdiņa

There are no investigations concerning the microstructural homogeneity in cross section of extruded and sintered samples found in literature. In this work TiO2 ceramics obtained by extrusion technology is investigated. Samples were sintered under three different sintering conditions: A) 1100→850 °C, B) 1100 °C and C) 1100→1450 °C. Two step sintering at 1100 – 850 °C leads to the formation of denser microstructure (77.2 % of TD) compared to single step sintering at 1100 °C (75.4 % of TD). After thermal treatment there are differences between microstructure in middle and edge part of all samples. Microstructure of samples after each sintering condition is different. Needle-shaped and irregularly shaped grains and bimodal porosity can be found in SEM investigations.


Atslēgas vārdi
TiO2, extrusion, theral treatment
DOI
10.1088/1757-899X/47/1/012019
Hipersaite
http://iopscience.iop.org/1757-899X/47/1/012019/pdf/1757-899X_47_1_012019.pdf

Pūra, A., Ločs, J., Bērziņa-Cimdiņa, L. The Effect of Thermal Processing Parameters on the Microstructure of Extruded and Sintered TiO2 Ceramics. IOP Conference Series: Materials Science and Engineering, 2013, Vol.47, Iss.1, 012019.-012019.lpp. ISSN 1757-8981. e-ISSN 1757-899X. Pieejams: doi:10.1088/1757-899X/47/1/012019

Publikācijas valoda
English (en)
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