Synthesis of 6‑Selanyl-2-triazolylpurine Derivatives Using 2,6-Bistriazolylpurines as Starting Materials
ACS Omega 2024
Agnija Ritere, Andris Jeminejs, Ērika Bizdēna, Māris Turks, Irina Novosjolova

Two pathways toward 6-selanyl-2-triazolylpurine derivatives were designed. The first method involved the synthesisof 2-chloro-6-selanylpurine derivatives, further SNAr reaction with NaN3, and following CuAAC using different alkynes. The secondmethod was based on the synthesis of 2,6-bistriazolylpurine derivatives as starting materials followed by SNAr reaction withcommercial or in situ generated selenols as nucleophiles. A series of 2-chloro-6-selanylpurine derivatives were obtained in yields upto 84%. It was found that in the latter compounds, 6-selanyl moiety was the better leaving group compared to 2-chlorosubstituent inSNAr reactions. On the other hand, the SNAr reaction between 2,6-bistriazolylpurines and selenols or diselenides was successful, and13 examples of 6-selanyl-2-triazolylpurine derivatives were obtained in yields up to 87%. This direct approach for the Se−C bondformation proved the ability of the 1,2,3-triazolyl ring at the C6 position of purine to act as a good leaving group.


Atslēgas vārdi
purine, selanylpurines, SNAr
DOI
10.1021/acsomega.3c04994
Hipersaite
https://pubs.acs.org/doi/10.1021/acsomega.3c04994

Ritere, A., Jeminejs, A., Bizdēna, Ē., Turks, M., Novosjolova, I. Synthesis of 6‑Selanyl-2-triazolylpurine Derivatives Using 2,6-Bistriazolylpurines as Starting Materials. ACS Omega, 2024, Vol. 9, No. 6, 6366.-6380.lpp. e-ISSN 2470-1343. Pieejams: doi:10.1021/acsomega.3c04994

Publikācijas valoda
English (en)
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